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Record W3130644662 · doi:10.1088/0026-1394/58/1a/08008

SIM.QM-S10: supplementary comparison for trace elements in skim milk powder

2021· article· en· W3130644662 on OpenAlexaffabout
Patrícia Grinberg, Zoltán Mester, Patricia Gatti, Osvaldo Reyes Acosta, Mabel Puelles, Mabel Delgado, Rodrigo Caciano de Sena, Marcelo Dominguez de Almeida, Márcia Silva da Rocha, Soraya Sandoval, Claudia Núñez, Javier Vera, Wei Chao, Xiao Li, Henry Torres Quezada, G. S. Torres, Diego A. Garzón, Diego A. Ahumada, Jimmy Venegas Padilla, Bryan Calderón-Jiménez, Evelyn Vasco, L Regalado Contreras, Mariana Arce Osuna, Radojko Jačimović, Tea Zuliani, Nunnapus Laitip, Usana Thiengmanee, Nattikarn Ornthai, Pranee Phukphatthanachai, Suttinun Taebunpakul, H Klich

Bibliographic record

VenueMetrologia · 2021
Typearticle
Languageen
FieldChemistry
TopicAnalytical chemistry methods development
Canadian institutionsNational Research Council Canada
Fundersnot available
KeywordsMutual recognitionMetrologyTraceabilityMathematicsTRACE (psycholinguistics)Statistics

Abstract

fetched live from OpenAlex

Main text SIM.QM-S10 was performed to assess the analytical capabilities of National Metrology Institutes (NMIs) and Designated Institutes (DIs) of SIM members (or other regions) for the accurate determination of trace metals in skim milk powder. The study was proposed by the coordinating laboratories National Research Council Canada (NRC) and INTI Argentina as an activity of Sistema Interamericano de Metrología (SIM) approved by the Inorganic Analysis Working Group (IAWG) of Consultative Committee for Amount of Substance - Metrology in Chemistry and Biology (CCQM). Participants included NMIs/DIs from twelve countries. No measurement method was prescribed by the coordinating laboratories. Therefore, NMIs used measurement methods of their choice. However, the majority of NMIs/DIs used closed vessel microwave system using a mixture of HNO 3 and H 2 O 2 for the digestion and ICP-MS and ICP-OES for the determination of the measurands. One laboratory used INAA technique. This SIM.QM-S10 Supplementary Comparison provides NMIs/DIs with the needed evidence for CMC claims for trace elements in skim milk powder and similar matrices. To reach the main text of this paper, click on Final Report . Note that this text is that which appears in Appendix B of the BIPM key comparison database kcdb.bipm.org/ . The final report has been peer-reviewed and approved for publication by the CCQM, according to the provisions of the CIPM Mutual Recognition Arrangement (CIPM MRA).

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.573
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0130.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.044
GPT teacher head0.344
Teacher spread0.300 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2021
Admission routes2
Has abstractyes

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