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Record W3151851393 · doi:10.1002/aesr.202100001

Translating Tactics from Direct CO<sub>2</sub> Electroreduction to Electroorganic Coupling Reactions with CO<sub>2</sub>

2021· article· en· W3151851393 on OpenAlex
Xenia Medvedeva, Jury J. Medvedev, Anna Klinkova

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueAdvanced Energy and Sustainability Research · 2021
Typearticle
Languageen
FieldEnergy
TopicCO2 Reduction Techniques and Catalysts
Canadian institutionsUniversity of Waterloo
FundersNatural Sciences and Engineering Research Council of CanadaCanada Foundation for InnovationOntario Research Foundation
KeywordsElectrosynthesisElectrochemical reduction of carbon dioxideNanotechnologyElectrochemistryCatalysisChemistryMaterials scienceOrganic chemistryElectrode

Abstract

fetched live from OpenAlex

Sustainable electrosynthesis technologies are rapidly developing stimulated by the drive for sustainable chemical manufacturing and the increasingly accessible renewable electricity prices. The electrochemical utilization of easily available feedstock, such as carbon dioxide (CO 2 ), has attracted significant attention as it can additionally help closing the disrupted carbon cycle. While direct CO 2 reduction has benefited from recent advancements in the catalyst, electrolyte and system design, developments in electrochemical coupling of CO 2 with organic precursors to yield value‐added chemicals have been lagging behind due to the apparent disconnect between the direct CO 2 reduction and the organic electrosynthesis communities. Currently, electrocarboxylation reactions require high operating voltages, show low current densities, limited selectivity towards target products and are associated with low atom economy due to the reliance on sacrificial anode dissolution. Advancing this indirect electrochemical CO 2 utilization strategy will enable sustainable synthesis of valuable chemicals including non‐steroidal anti‐inflammatory drugs and precursors for plasticizers and commercially‐relevant polymers—all of which are currently produced with high carbon footprint and low atom economy. This perspective discusses the current state‐of‐the‐art in electroorganic synthesis with CO 2 as a one‐carbon synthon and suggests several transferrable strategies from direct CO 2 reduction breakthroughs to advance electrocarboxylation and bring it closer to industrial implementation.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.132
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.002
Science and technology studies0.0010.000
Scholarly communication0.0000.001
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.014
GPT teacher head0.309
Teacher spread0.295 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it