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Record W3159271740 · doi:10.1002/jsde.12510

Phase Behavior of Non‐Ionic <scp>Surfactant‐Medium</scp> Chain <scp>Triglyceride‐Water</scp> Microemulsion Systems

2021· article· en· W3159271740 on OpenAlexafffund
Shannon P. Callender, Shawn Wettig

Bibliographic record

VenueJournal of Surfactants and Detergents · 2021
Typearticle
Languageen
FieldChemistry
TopicSurfactants and Colloidal Systems
Canadian institutionsUniversity of Waterloo
FundersNatural Sciences and Engineering Research Council of CanadaMitacs
KeywordsMicroemulsionChemistryPulmonary surfactantSolubilityDrug deliveryPolyethylene glycolChromatographyPolysorbateOrganic chemistryChemical engineering

Abstract

fetched live from OpenAlex

Abstract Microemulsion systems have garnered tremendous interest in the pharmaceutical sector for a variety of drug delivery applications. Non‐ionic surfactants are often the preferred surfactant class given their uncharged nature, enhanced oral safety profile, and generally regarded as safe status as compared to other surfactant classes (Myers, Surfactant science and technology, 2005, p. 29), (Malmsten, Handbook of microemulsion science and technology, 1999, p. 755), (Grove &amp; Mullertz, Chapter 5‐liquid self‐microemulsifying drug delivery systems, 2007), (Liu et al., Water‐insoluble drug formulation, 2008), (Hauss, Advanced Drug Delivery Reviews, 2007, 59, pp. 667–676), (Balazs, Solubility, delivery and ADME problems of drugs and drug‐candidates, 2011, p. 68). In this work, the phase behavior and microemulsion formation potential of four commonly used non‐ionic surfactants, PEG‐40 hydrogenated castor oil, Poloxamer 188, Polysorbate 80, and d ‐α‐tocopherol polyethylene glycol succinate were studied via ternary phase diagram (TPD) mapping using a medium chain triglyceride, Miglyol 812. Results indicated notable differences in phase behavior despite similarities in hydrophilic–lipophilic balance value (13–15). All surfactants produced Winsor Type I, oil‐in‐water microemulsions at water concentrations above 40% wt/wt. Winsor Type II water‐in‐oil microemulsions were difficult to obtain even at high oil concentrations of ≥70% wt/wt. Winsor III microemulsions, though rare, were generally obtained in the middle regions of the TPD between 10% and 30% wt/wt water while Winsor IV microemulsions dominated at high surfactant concentrations of ≥45% wt/wt. Opaque emulsion areas were particularly notable in wax state surfactants. Polysorbate 80 and PEG‐40 hydrogenated castor oil demonstrated a high degree of synergism as well as the largest oil‐in‐water (o/w) and water‐in‐oil (w/o) microemulsion formation potential rendering them suitable for a number of enteral and parenteral applications.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.042
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0020.001
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0010.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.016
GPT teacher head0.259
Teacher spread0.243 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations18
Published2021
Admission routes2
Has abstractyes

Explore more

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