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Lithium Ytterbium-Based Halide Solid Electrolytes for High Voltage All-Solid-State Batteries

2021· article· en· W3172826361 on OpenAlex
Se Young Kim, Kavish Kaup, Kern Ho Park, Abdeljalil Assoud, Laidong Zhou, Jue Liu, Xiaohan Wu, Linda F. Nazar

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueACS Materials Letters · 2021
Typearticle
Languageen
FieldEngineering
TopicAdvanced Battery Materials and Technologies
Canadian institutionsUniversity of Waterloo
FundersNatural Sciences and Engineering Research Council of CanadaCanada Research ChairsBASF
KeywordsElectrolyteFast ion conductorMaterials scienceHalideIonic conductivityElectrochemistryCathodeSulfideInorganic chemistryLithium (medication)Chemical engineeringChemistryPhysical chemistryMetallurgyElectrode

Abstract

fetched live from OpenAlex

All-solid-state Li-ion batteries that utilize nonflammable solid electrolytes are considered potential candidates for sustainable energy storage systems. Although sulfide solid electrolytes have been widely explored, their lack of electrochemical stability above 2.7 V requires the application of protective coating layer on 4 V-class cathode materials, whereas the superior oxidative stability of chloride solid electrolytes enables their direct use with such high voltage cathodes. Here, we report a metastable trigonal phase of Li3YbCl6 with an ionic conductivity of 1.0 × 10–4 S·cm–1 and mixed-metal halide solid electrolytes, Li3–xYb1–xZrxCl6, with conductivities up to 1.1 mS·cm–1 at room temperature. Combined neutron, single-crystal, and powder X-ray diffraction methods reveal that Zr-substitution for Yb in Li3YbCl6 triggers a trigonal-to-orthorhombic phase transition and forms new, lower energy pathways for Li-ion migration. All-solid-state cell cycling with uncoated >4 V-class cathodes is enabled by the high electrochemical oxidation stability of the mixed-metal halide solid electrolyte.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.033
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.229
Teacher spread0.220 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it