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Record W3189308233 · doi:10.1038/s43246-021-00187-2

Reducing crystallinity in solid polymer electrolytes for lithium-metal batteries via statistical copolymerization

2021· article· en· W3189308233 on OpenAlexafffund
Vincent St‐Onge, Mengyang Cui, Sylviane Rochon, Jean‐Christophe Daigle, Jérôme P. Claverie

Bibliographic record

VenueCommunications Materials · 2021
Typearticle
Languageen
FieldEngineering
TopicAdvanced Battery Materials and Technologies
Canadian institutionsMcMaster UniversityUniversité de Sherbrooke
FundersNatural Sciences and Engineering Research Council of CanadaMitacsHydro-QuébecMcMaster University
KeywordsComonomerCrystallinityIonic conductivityMaterials scienceEthylene oxideElectrolytePolymerLithium (medication)Chemical engineeringCopolymerOxidePolymer chemistryConductivityChemistryComposite materialPhysical chemistryElectrodeMetallurgyMedicine

Abstract

fetched live from OpenAlex

Abstract The discovery that polyethylene oxide promotes ionic conductivity led to the development of solid polymer electrolytes. However, their conductivity is severely reduced by crystallinity. Here, statistical copolymerization is used to design macromolecular architectures where crystallinity is disrupted by a minimal amount of non-ethylene oxide comonomer units. Using the Flory exclusion model, we demonstrate that polymers containing 18 mol% comonomer and 18 wt% LiTFSI are devoid of crystallinity. A 10 mol% comonomer content is sufficient to reach a conductivity of 0.3 × 10 −4 S cm −1 at 25 °C. The Li + transference number is 0.6, indicating that the comonomer units not only limit the crystallinity but also weaken the strength of the Li + coordination to the polymer. The resulting solid polymer electrolyte is effective in an all-solid LFP|Li-metal battery operating at 25 °C, demonstrating that statistical copolymerization is an efficient tool for polymer electrolyte design.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.004

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.020
GPT teacher head0.280
Teacher spread0.260 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations106
Published2021
Admission routes2
Has abstractyes

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