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Detection of heart-fatty acid binding protein in human serum using gold nano/micro-islands and molecularly imprinted polymers

2021· article· en· W3197430754 on OpenAlexaff
Alireza Sanati, Roozbeh Siavash Moakhar, K. Raeissi, Fathallah Karimzadeh, Hojatollah Vali, Sara Mahshid

Bibliographic record

Venuenot available
Typearticle
Languageen
FieldChemistry
TopicElectrochemical Analysis and Applications
Canadian institutionsMcGill University
Fundersnot available
KeywordsMolecularly imprinted polymerDifferential pulse voltammetryDetection limitBiosensorMyoglobinPolymerChemistryCyclic voltammetryCombinatorial chemistryMaterials scienceChromatographyAnalytical Chemistry (journal)NanotechnologyElectrodeSelectivityElectrochemistryBiochemistryOrganic chemistryPhysical chemistry

Abstract

fetched live from OpenAlex

Here, we have developed a biomimetic sensor using gold nano/micro-islands (NMIs) and molecularly imprinted polymers (MIPs) for electrochemical detection of H-FABP. The fabricated nanostructured electrode was characterized and its analytical performance was evaluated in human serum spiked with H-FABP in the clinical range (10 pg mL <sup xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">−1</sup> to 100 ng mL <sup xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">−1</sup> ). In this regard, an excellent linear performance (R2=0.99) and a low limit of detection (LOD) of 4.86 pg mL <sup xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">−1</sup> were observed. Moreover, the selectivity performance of the proposed biosensor was investigated in the presence of troponin T (TnT), and myoglobin (Myo). The differential pulse voltammetry (DPV) results showed that the MIP current has altered approximately 16, 20, and 62% for TnT, Myo, and H-FABP, respectively, confirming the low interference of other cardiac biomarkers on the sensing performance. Ultimately, the developed biomimetic sensor fabricated by the integration of hierarchical structures of gold and MIP opens up future perspectives for sensitive, low-cost, and early detection of myocardial infarction in human serum.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.384

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.239
Teacher spread0.231 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations3
Published2021
Admission routes1
Has abstractyes

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