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Record W3204566432 · doi:10.26434/chemrxiv.12268622.v1

Bi Is the New B: High Lewis acidity at a planar, trivalent, neutral, electropositive p-block element

2020· preprint· en· W3204566432 on OpenAlexafffund
Katherine M. Marczenko, Samantha Jee, Saurabh S. Chitnis

Bibliographic record

VenueChemRxiv · 2020
Typepreprint
Languageen
FieldChemistry
TopicOrganoboron and organosilicon chemistry
Canadian institutionsDalhousie University
FundersNatural Sciences and Engineering Research Council of CanadaDalhousie UniversityNova Scotia Research Innovation Trust
KeywordsLewis acids and basesBismuthChemistryPlanarIonFluorideElectrophileLewis acid catalysisElectronegativityInorganic chemistryComputational chemistryCatalysisOrganic chemistryComputer science

Abstract

fetched live from OpenAlex

Geometric perturbation away from VSEPR-predicted structures can engender unusual frontier MO situations leading to high Lewis acidity. Recently we reported a T-shaped bismuth triamide, which exhibited planar Lewis acidity that was unprecedented for neutral Group 15 compounds. We now report a comprehensive computational assessment of the origins of planar Lewis acidity in such compounds. We subsequently use several metrics such as MO energies, the Global Electrophilicity Index, ligand coordination strengths, and Fluoride Ion Affinity to show that electronic variation can be combined with the unusual geometry at bismuth to achieve fine tuning of Lewis acid strength. Our calculations reveal for the first time a surprisingly high Lewis acidity – comparable to or exceeding that of polyfluorinated triarylboranes – as well as high rigidity at neutral planar bismuth triamides. These results foreshadow the potentially broad applications of a hitherto unexplored class of compounds – planar bismuthanes – in several contexts such as anion sensing, Lewis acid catalysis, weakly-coordinating anion chemistry and materials science that are currently dominated by Lewis acidic triarylboranes.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.009
Threshold uncertainty score0.030

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0010.001
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0090.002

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.019
GPT teacher head0.246
Teacher spread0.227 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2020
Admission routes2
Has abstractyes

Explore more

Same venueChemRxiv→Same topicOrganoboron and organosilicon chemistry→French-language works237,207→