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Sistemas aquosos bifásicos de polietilenoglicol e sais inorgânicos

2015· dissertation· pt· W4205908306 on OpenAlexaff
Filipe Leôncio Braga

Bibliographic record

Venuenot available
Typedissertation
Languagept
FieldChemistry
TopicSurfactants and Colloidal Systems
Canadian institutionsDiscovery Air (Canada)
Fundersnot available
KeywordsAqueous solutionPolymerThermodynamicsMoleculeHydrogen bondChemistryMonomerMaterials sciencePolymer chemistryChemical physicsPhysical chemistryPhysicsOrganic chemistry

Abstract

fetched live from OpenAlex

Thermal-statistical models that try to reproduce the behavior of aqueous polymer solutions have been extensively studied over the years. However, the number of articles related to aqueous systems containing polymers and added salts is still very restricted. Across the developed thesis, we work within the Flory-Huggins theory framework to model the formation of aqueous two-phase systems containing long-polymer chains of polyethylene-glycol in mixtures containing monovalent inorganic salts. Within the model, the competition between the hydrogen-bond formation between water molecules and the monomers of the polymer chain, in addition to the ion-dipole interactions between water molecules and the dissociated salt ions, play a key role in shaping equilibrium congurations. Through numerical ts of experimental data for each salt type introduced into the mixture with model predictions for the lowest temperatures for the formation of two phases, so-called Cloud Point Temperature (CPT), we nd a set of four interaction parameters that enables proper representation of the continuous behavior of CPTs as a function of the solutes concentration.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Research integrity, Insufficient payload (model declined to judge)
Consensus categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.272
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0020.001
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0010.000
Open science0.0010.000
Research integrity0.0020.001
Insufficient payload (model declined to judge)0.0090.003

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.023
GPT teacher head0.290
Teacher spread0.267 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; both teacher heads agree on what is shown here.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2015
Admission routes1
Has abstractyes

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