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Viability of Boron Nitride Nanotubes as a Support Structure for Metal Nanoparticle Catalysts for the Plasma-Catalytic Synthesis of Ammonia

2021· article· en· W4207014396 on OpenAlexafffund
S. Brett Walker, Gareth D. Price, Elmira Pajootan, Sylvain Coulombe

Bibliographic record

Venuenot available
Typearticle
Languageen
FieldChemical Engineering
TopicAmmonia Synthesis and Nitrogen Reduction
Canadian institutionsMcGill University
FundersNational Research Council Canada
KeywordsNanomaterial-based catalystBoron nitrideCatalysisMaterials scienceNanoparticleChemical engineeringSurface modificationNanotechnologyOrganic chemistryChemistry

Abstract

fetched live from OpenAlex

Nonthermal plasma-catalytic processes are being investigated as an alternative method to the energy-intensive and environmentally impactful Haber-Bosch (H-B) process for ammonia synthesis. Due to the large-scale production of this commodity chemical, the H-B process uses 1-2% of the world's energy, 3-5% of the world's refined natural gas and corresponding CO <inf xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">2</inf> emissions. With the recent development of large-scale electrolysers for H <inf xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">2</inf> production powered by renewable electricity, the integration of a plasma process at scale may be the last step toward the all-electric and environment-friendly green ammonia synthesis. However, the most encouraging results are still an order of magnitude below the H-B process in terms of energy efficiency. Key to success are the nanocatalysts, the plasma excitation and gas mixing, with reaction kinetics as the coupling between these variables. Boron nitride nanotubes (BNNTs) are a dielectric material with high chemical and thermal stability, and a unique affinity to ammonia. These properties make them interesting substrates for nanocatalysts. We report on the surface modification of BNNTs and the deposition of metal catalyst nanoparticles by two sequential plasma processing steps; plasma functionalization and pulsed laser ablation to produce BNNT-supported nanoparticle catalysts. We also report our additional findings on the morphology, activity, and stability of the produced catalysts.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.002
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.006
Threshold uncertainty score0.523

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.002
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.012
GPT teacher head0.239
Teacher spread0.227 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2021
Admission routes2
Has abstractyes

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