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Record W4210948953 · doi:10.1002/9780470027318.a8105m

Microwave Techniques

2000· other· en· W4210948953 on OpenAlex
Frank E. Smith, Guohua Xiong

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueEncyclopedia of Analytical Chemistry · 2000
Typeother
Languageen
FieldChemistry
TopicMicrowave-Assisted Synthesis and Applications
Canadian institutionsLaurentian University
Fundersnot available
KeywordsInstrumentation (computer programming)Management scienceComputer scienceNanotechnologyBiochemical engineeringProcess engineeringData scienceEngineeringMaterials science

Abstract

fetched live from OpenAlex

Abstract A concise yet comprehensive review of the use of microwave‐assisted techniques for sample preparation in analytical chemistry is presented. A historical review of the development of the field is followed by summaries of the most significant theoretical principles, available instrumentation and safety considerations. The major part of the review concerns recent applications of the techniques to the preparation of a wide range of sample types. These include environmental, soil, biological, clinical, food, pharmaceutical, mineral, ceramic and industrial samples. Examples of microwave‐assisted drying and fusion of analytical samples are also given. Throughout, reference is made to the most important review articles. Where appropriate, original papers are summarized and cited.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Not applicable · Consensus signal: Not applicable
GenreCandidate signal: Other · Consensus signal: Other
Teacher disagreement score0.114
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0010.000
Insufficient payload (model declined to judge)0.1140.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.238
Teacher spread0.230 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it