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Record W4211233332 · doi:10.32920/ryerson.14657796.v1

Solubility measurement of polyethylene glycol polymers in supercritical carbon dioxide at high pressures and temperatures

2021· preprint· en· W4211233332 on OpenAlexaff
Kamal Al Rafea

Bibliographic record

Venuenot available
Typepreprint
Languageen
FieldEngineering
TopicPhase Equilibria and Thermodynamics
Canadian institutionsToronto Metropolitan University
Fundersnot available
KeywordsSupercritical fluidSolubilitySupercritical carbon dioxidePolymerChemical engineeringSolventPolyethylene glycolSupercritical fluid extractionOrganic chemistryCarbon dioxideChemistrySupercritical water oxidationMaterials science

Abstract

fetched live from OpenAlex

Solubility and its measurement of different materials including polymers, drugs, proteins, peptides and many other organic or non organic compounds in supercritical fluids are of great importance in a wide variety of applications. These applications include: production of controlled drug delivery systems, powder processing, pollution prevention, spraying paints and coatings, and food processing. Supercritical Fluids are fetting more interest since the last two decades due to their abilities in replacing VOC solvents, and because of their tunable properties that could be achieved by varying their pressure and temperature in getting powerful solvents. Supercritical fluid is a substance under pressure absove its critical temperature. Under supercritical conditions the distinction between gases and liquids does not apply and substance can only be described as a fluid. Supercritical fluids have properties intermediate between those of gases and liquids, controlled by the pressure. They do not condense or evaporate to form a liquid or a gas. Fluids such as supercritical carbon dioxide offer a range of unusual chemical possibilities in both synthetic and analytical chemistry. Supercritical fluids have solvent power similar to a light hydrocarbon for most solutes.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.005

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.002
Science and technology studies0.0000.001
Scholarly communication0.0000.001
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0020.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.011
GPT teacher head0.213
Teacher spread0.202 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2021
Admission routes1
Has abstractyes

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