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Record W4213278572 · doi:10.1021/acs.chemmater.1c04055

Elucidating the Role of Hydrogen Bonds for Improved Mechanical Properties in a High-Performance Semiconducting Polymer

2022· article· en· W4213278572 on OpenAlexafffund
Luke Galuska, Michael U. Ocheje, Zachary Ahmad, Simon Rondeau‐Gagné, Xiaodan Gu

Bibliographic record

VenueChemistry of Materials · 2022
Typearticle
Languageen
FieldEngineering
TopicAdvanced Sensor and Energy Harvesting Materials
Canadian institutionsUniversity of Windsor
FundersDivision of Materials ResearchNatural Sciences and Engineering Research Council of Canada
KeywordsPolymerMaterials scienceHydrogen bondSurface modificationConjugated systemUltimate tensile strengthDuctility (Earth science)AmideIntermolecular forceBond strengthChemical engineeringPolymer chemistryComposite materialNanotechnologyChemistryOrganic chemistryMoleculeAdhesive

Abstract

fetched live from OpenAlex

Incorporation of hydrogen bond moieties into the backbone or side chain of conjugated polymers is an effective strategy to enhance mechanical performance, facilitate morphological organization, and promote self-healing ability. However, the understanding of hydrogen bonds, particularly the effect of bond strength and directionality, on thermomechanical and optoelectronic performance is still in its infancy due to the competing influence of morphology, glass transition phenomena, and the measurement process itself. Here, we compare the influence of statistically incorporated amide and urea moieties on the mechanical properties of DPP-TVT parent polymers. We observed a profound difference in ductility; amide functionalization increases the strain at failure by over 100% relative to the pure DPP-TVT polymer, while urea functionalization results in a loss of strain at failure by 50%. This is attributed to the crystalline behavior of functionalized conjugated polymers that is promoted by intermolecular interactions of urea groups, which we elucidated via an in-depth investigation of the swelling, crystalline packing, thermal behavior, and strain-dependent charge transport. Furthermore, we employed a novel free-standing tensile test to validate our mechanical measurements supported on a water surface. Our results demonstrated that hydrogen bond moieties must be carefully chosen to achieve a delicate balance of morphological control and mechanical performance, as simply increasing the hydrogen bond strength can result in detrimental mechanical and electrical performance.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.018
Threshold uncertainty score0.416

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.011
GPT teacher head0.194
Teacher spread0.183 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations74
Published2022
Admission routes2
Has abstractyes

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