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Effect of forging temperature on the structure, mechanical and functional properties of superelastic Ti-Zr-Nb bar stock for biomedical applications

2022· article· en· W4214882537 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueLetters on Materials · 2022
Typearticle
Languageen
FieldMaterials Science
TopicTitanium Alloys Microstructure and Properties
Canadian institutionsÉcole de Technologie Supérieure
FundersRussian Science Foundation
KeywordsMaterials scienceSubstructureAlloyForgingComposite materialGrain sizeVolume fractionModulusElastic modulusMicrostructureShear modulusMetallurgyStructural engineering

Abstract

fetched live from OpenAlex

Ti-Zr-Nb shape memory alloys exhibit a unique combination of properties that make them suitable for bone implants: low Young’s modulus, superelastic behavior, superior corrosion resistance, and non-toxicity of all the constitutive elements. In this study, superelastic Ti-19Zr-14Nb (at.%) alloy was subjected to a combination of radial shear rolling at 900°C and rotary forging in a temperature range from 500 to 700°C to form long-length bar stocks for bone implants fabrication. Features of the grain structure, phase composition, mechanical and functional properties of the long-length bar stocks were analyzed using light microscopy, X-ray analysis, as well as during mechanical and functional tests. It was shown that after radial shear rolling at 900°C, a heterogeneous grain structure was formed over the cross-section of the bar stock, and this structure was inherited after the subsequent rotary forging at 500°C. With an increase in the forging temperature, the structural heterogeneity is eliminated and the grain size increases, while the hardness and strength characteristics of the material decrease. After rotary forging at 700°C, the alloy manifests the best combination of structural, mechanical, and functional characteristics. In this state, the long-length bar stock demonstrates a homogeneous grain structure with a certain fraction of a dynamically polygonized substructure of β-phase, a satisfactory strength (UTS ≈ 580 MPa), a low Young’s modulus (E ≈ 35 GPa), the high difference between dislocation and phase yield strength (Δσ ≈ 280 MPa), and a relatively large amount of superelastic recovery strain (εrSEmax ≈ 3.1%).

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.807

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.012
GPT teacher head0.212
Teacher spread0.200 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it