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Record W4243467974 · doi:10.1002/047084289x.ra079

Aluminum Chloride

2005· reference-entry· en· W4243467974 on OpenAlexaff
Paul Galatsis, Krishnakumar Ranganathan

Bibliographic record

VenueEncyclopedia of Reagents for Organic Synthesis · 2005
Typereference-entry
Languageen
FieldChemistry
TopicOrganic and Inorganic Chemical Reactions
Canadian institutionsUniversity of Guelph
Fundersnot available
KeywordsNitrobenzeneChemistryChlorideChloroformMethyleneBenzeneNitromethaneCarbon disulfideCatalysisOdorOrganic chemistrySolubilityNuclear chemistryMedicinal chemistry

Abstract

fetched live from OpenAlex

[7446-70-0] AlCl3 (MW 133.34) InChI = 1S/Al.3ClH/h;3*1H/q+3;;;/p-3 InChIKey = VSCWAEJMTAWNJL-UHFFFAOYSA-K (Lewis acid catalyst for Friedel–Crafts, Diels–Alder, [2 + 2] cycloadditions, ene reactions, rearrangements, and other reactions) Physical Data: mp 190 °C (193–194 °C sealed tube); sublimes at 180 °C; d 2.44 g cm−3. Solubility: sol many organic solvents, e.g. benzene, nitrobenzene, carbon tetrachloride, chloroform, methylene chloride, nitromethane, and 1,2-dichloroethane; insol carbon disulfide. Form Supplied in: colorless solid when pure, typically a gray or yellow-green solid; also available as a 1.0 M nitrobenzene solution. Handling, Storage, and Precautions: fumes in air with a strong odor of HCl. AlCl3 reacts violently with H2O. All containers should be kept tightly closed and protected from moisture.1c Use in a fume hood.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Not applicable · Consensus signal: none
GenreCandidate signal: Other · Consensus signal: Other
Teacher disagreement score0.211
Threshold uncertainty score0.706

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0030.001
Meta-epidemiology (broad)0.0020.001
Bibliometrics0.0020.002
Science and technology studies0.0010.000
Scholarly communication0.0010.001
Open science0.0030.001
Research integrity0.0010.002
Insufficient payload (model declined to judge)0.2110.209

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.015
GPT teacher head0.244
Teacher spread0.229 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designNot applicable
Domainnot available
GenreOther

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2005
Admission routes1
Has abstractyes

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