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Record W4249127470 · doi:10.15278/isms.2021.rd03

THE 4.2 MICRON SPECTRA OF CO<sub>2</sub>-CO DIMER FOR BOTH THE C- AND O-BONDED ISOMERS, INCLUDING SPLITTING OF THE DEGENERATE ν<sub>2</sub> BEND IN THE PRESENCE OF CO

2021· article· en· W4249127470 on OpenAlexaff
Praveen Wakwella, Nasser Moazzen-Ahmadi, Bob McKellar, A. Barclay

Bibliographic record

VenueProceedings of the 2021 International Symposium on Molecular Spectroscopy · 2021
Typearticle
Languageen
FieldChemistry
TopicAnalytical Chemistry and Chromatography
Canadian institutionsUniversity of Calgary
Fundersnot available
KeywordsDegenerate energy levelsDimerSpectral lineMaterials scienceCrystallographyChemistryPhysicsNuclear magnetic resonanceQuantum mechanics

Abstract

fetched live from OpenAlex

CO$_2$-CO dimer was previously observed by high-resolution microwave and infrared spectroscopy in the form of a planar T-shaped C-bonded structure.\\footnote{A.C. Legon, A.P. Suckley, \\textit{Journal of Chemical Physics} \\textbf{91} 4440 (1989).}$^,$\\footnote{R.W. Randall, J.P.L. Summersgill, B.J. Howard, \\textit{Journal Chemical Society Faraday Transactions} \\textit{86} 1943 (1990).} More recently, spectra of a second isomer were observed in the stretching region of carbon monoxide.\\footnote{S. Sheybani-Deloui, A.J. Barclay, K.H. Michaelian, A.R.W. McKellar, N. Moazzen-Ahmadi, \\textit{Journal of Chemical Physics} \\textbf{143} 121101 (2015).} This isomer has also a planar T-shaped structure, but with the CO flipped by $180^{\\circ}$. Moreover, two intermolecular frequencies were measured for each isomer. These are in very good agreement with recent high level theoretical calculations.\\\\ \nHere, CO$_2$-CO dimer is observed in the carbon dioxide $\\nu_3$ asymmetric stretch region ($\\sim$2350 cm$^{-1}$). Both C-bonded and O-bonded isomers are analyzed for the normal isotopologue as well as for $^{13}$CO$_2$-CO and $^{16}$O$^{13}$C$^{18}$O-CO, the latter being the first observation of an asymmetrically substituted form for which all values of K$_a$ are allowed. Combination bands involving the lowest in-plane intermolecular mode are also observed yielding frequencies of 24.51 \\wn for the C-bonded form and 14.37 \\wn for the O-bonded form. \nIn addition, two weak bands near 2337 \\wn are assigned to CO$_2$ hot band transitions (01$^{1}$1) - (01$^{1}$0), yielding the splitting of the degenerate CO$_2$ bend into in-plane and out-of-plane components due to the presence of the CO. This splitting has rather different values for the C- and O- bonded isomers, 4.56 and 1.59 \\wn, respectively, with the out-of-plane mode higher in energy than the in-plane for both cases.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.017
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0000.001
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0020.001
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.260
Teacher spread0.251 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2021
Admission routes1
Has abstractyes

Explore more

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