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Record W4250069833 · doi:10.26434/chemrxiv.12355847

Oxygen Redox Activity in Cathodes – a Common Phenomenon Calling for Density-Based Descriptors

2020· preprint· en· W4250069833 on OpenAlexaff
Daniel Koch, Sergei Manzhos

Bibliographic record

VenueChemRxiv · 2020
Typepreprint
Languageen
FieldEnergy
TopicElectrocatalysts for Energy Conversion
Canadian institutionsInstitut National de la Recherche Scientifique
Fundersnot available
KeywordsRedoxChemical physicsDensity functional theoryOxideChemistryTransition metalOxygenCharge densityComputational chemistryPhysicsInorganic chemistryQuantum mechanicsCatalysisOrganic chemistry

Abstract

fetched live from OpenAlex

Lithium-excess transition metal oxide materials are promising cathode candidates for future secondary batteries due to their relatively high energy density, which is commonly related to redox-active oxygen centers. First-principle computations are crucial for the understanding of the underlying redox mechanism in these compounds, with plane-wave density functional theory being the most frequently used setup. An important tool for the assignment of the redox-active species is the projected density of states, although the atomic contributions postulated this way do not strictly correspond to any observable physical quantity. By directly analyzing the computed real-space charge density changes, on the other hand, oxygen redox activity can be found to be substantial in most transition metal oxide compounds, although a projection onto atomic states would suggest otherwise. This can be linked to the shortcomings of the commonly employed spherical approximation for ions in crystalline compounds used to compute the projected density of states, which fails to describe the charge density topology in covalent transition metal oxides and leads to a qualitatively different picture from a charge density-based approach, specifically, the underrepresentation of oxygen contributions and exaggeration of transition metal contributions to the density of states The density based approach, due to the non-spherical nature of Bader domains, is more apt to properly describe oxygen redox contributions. This raises the question how meaningful the descriptors of oxygen redox activity are and how it should be acknowledged for transition metal oxide compounds in general.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.002
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Simulation or modeling · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: none
Teacher disagreement score0.002
Threshold uncertainty score0.008

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0010.002
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.001
Science and technology studies0.0000.001
Scholarly communication0.0010.002
Open science0.0010.001
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0020.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.036
GPT teacher head0.261
Teacher spread0.225 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designSimulation or modeling
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2020
Admission routes1
Has abstractyes

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