MétaCan
Menu
Back to cohort
Record W4285592441 · doi:10.1002/cjce.24552

Recovery of valeric acid using green solvents

2022· article· en· W4285592441 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

venuePublished in a venue whose home country is Canada.
no affNo Canadian affiliation: this work is invisible to an affiliation-only frame.
No Canadian affiliation. An affiliation-only frame, the usual design, would never have seen this work. It is one of the works that make the case for inverting the frame.

Bibliographic record

VenueThe Canadian Journal of Chemical Engineering · 2022
Typearticle
Languageen
FieldEngineering
TopicExtraction and Separation Processes
Canadian institutionsnot available
Fundersnot available
KeywordsDiluentChemistrySunflower oilSunflowerSoybean oilExtraction (chemistry)StoichiometryExothermic reactionValeric acidDilutionEnthalpyPartition coefficientNuclear chemistryChromatographyOrganic chemistryAcetic acidFood scienceAgronomy

Abstract

fetched live from OpenAlex

Abstract In this work, extraction of valeric acid (VA) using tri‐ n ‐butyl phosphate (TBP) as a reactive extractant was carried out. To reduce the toxic effects of the conventional diluents on microorganisms, non‐toxic and green edible sunflower and soybean oils were tried as the diluents. The high values of the distribution coefficient and extraction efficiency advocated to use them in the bio‐refinery industries. Moreover, it shows intensification of the recovery of VA using reactive extraction process. Sunflower oil appeared to be a better diluent than soybean oil. The complexation reaction stoichiometry ( m and n ) and equilibrium complexation reaction constant were estimated by using the differential evolution technique. In spite of the loading ratio being less than 0.5, the estimated m/n was found to be more than 1.0. The higher values of occurred due to the 9higher stability of the VA‐TBP complex in sunflower oil than in soybean oil. The stoichiometry of VA decreased with increasing TBP concentration. The complex concentration, , was found to be higher for soybean oil. It increased with temperature and initial VA concentration but remained invariant with TBP concentration. Due to the decreasing trend of with temperature, the complexation reaction became exothermic. The enthalpy changes due to mass transfer stipulated easier mixing of the phases in sunflower oil than in soybean oil.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Simulation or modeling · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.357
Threshold uncertainty score0.262

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.016
GPT teacher head0.206
Teacher spread0.190 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it