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Record W4285596338 · doi:10.1002/cjce.24549

Design and development of a simple and highly sensitive <scp>anthocyanin‐based</scp> sensing device for colorimetric urea determination

2022· article· en· W4285596338 on OpenAlexafffundvenue
Shamshad Ul Haq, Maryam Aghajamali, Hassan Hassanzadeh

Bibliographic record

VenueThe Canadian Journal of Chemical Engineering · 2022
Typearticle
Languageen
FieldEngineering
TopicAdvanced Chemical Sensor Technologies
Canadian institutionsUniversity of Calgary
FundersCanadian Network for Research and Innovation in Machining Technology, Natural Sciences and Engineering Research Council of CanadaUniversity of Calgary
KeywordsUreaseUreaDetection limitChemistryAnthocyaninHydrolysisAmmoniaSpectrophotometryChromatographyAmmonia volatilization from ureaSolventBiochemistryFood science

Abstract

fetched live from OpenAlex

Abstract We introduce a rapid anthocyanin‐based paper sensor with very high sensitivity and optical visibility for colorimetric detection of urea. The working principle is based on a colour change from purple to blue upon sensor exposure to ammonia generated from urea hydrolysis in the presence of urease as a catalyst. To improve sensor sensitivity and optical visibility, anthocyanin storage, urease solvent, urea hydrolysis time, and temperature were investigated. The results indicated that the anthocyanin extracted from red cabbage and stored in dark and low‐temperature conditions, urease extracted into water55 + glycerol45 (Aq55 + G45), and urea hydrolysis time of 40 min and temperature of 45°C offer the best detection condition. The fabricated sensor showed exceptional sensitivity of 0.018 pixel/mg urea‐N/L with a very low limit of detection (2.01 mg urea‐N/L) and a limit of quantification (6.71 mg urea‐N/L). Moreover, the sensor reaction zone is optically visible for urea concentration as low as 5 mg urea‐N/L, making it a promising tool for urea screening in diverse applications. The unique analytical features and accuracy of the sensor compared to the spectrophotometry method also suggest that it can be used as a replacement for environmentally unfriendly spectrophotometry methods for on‐site urea determination.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Methods · Consensus signal: none
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0010.000
Research integrity0.0010.000
Insufficient payload (model declined to judge)0.0010.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.016
GPT teacher head0.205
Teacher spread0.189 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreMethods

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

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Citations1
Published2022
Admission routes3
Has abstractyes

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