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Record W4296184854 · doi:10.1002/app.53144

Polyacrylic acid <scp>ultra‐thin</scp> films: Influence of <scp>cross‐linking</scp> structure via hyperthermal hydrogen‐induced cross‐linking

2022· article· en· W4296184854 on OpenAlexaff
Mengfan Liang, Yan Zhu, Run Xu, Junqiang Wang, Jian Cui, De‐Quan Yang, Heng‐Yong Nie, Woon‐Ming Lau

Bibliographic record

VenueJournal of Applied Polymer Science · 2022
Typearticle
Languageen
FieldEngineering
TopicSemiconductor materials and devices
Canadian institutionsWestern University
FundersNational Natural Science Foundation of China
KeywordsX-ray photoelectron spectroscopyPolyacrylic acidContact angleAcrylic acidHydrogen bondPolymerPolymer chemistryMaterials scienceChemical engineeringPolylactic acidSurface modificationChemistryOrganic chemistryMoleculeCopolymerComposite material

Abstract

fetched live from OpenAlex

Abstract The facile technology of hyperthermal hydrogen‐induced cross‐linking (HHIC) has recently been employed to efficiently cross‐link the typical surface modification material of poly acrylic acid (PAA) on polymer substrates, such as polylactic acid substrates, parylene C substrates and hydrophobic polypropylene substrates. This paper systematically studied the HHIC induced self‐cross‐linking of PAA without polymer substrates. It was found that the H was cleaved not only from the CH, but also from the surface functional group COOH, evidenced by both X‐ray photoelectron spectroscopy (XPS) measurement and the water contact angle test. We explained the self‐cross‐linking process as a result of both CC bonding and COOC bonding. Meanwhile, it was also found that PAA on different substrates can also be cross‐linked by secondary electron generated by X‐ray radiation during XPS analysis, which could be the main reason for wide variations of different reported XPS results.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.046
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0010.001
Science and technology studies0.0010.001
Scholarly communication0.0000.001
Open science0.0020.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.229
Teacher spread0.220 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations4
Published2022
Admission routes1
Has abstractyes

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