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Record W4310181384 · doi:10.26434/chemrxiv-2022-g4zj8

Challenging the Activity-Durability Tradeoff of Fe-N-C Fuel Cell Catalysts via Controlling thermal Activation Atmosphere

2022· preprint· en· W4310181384 on OpenAlexaff
Yachao Zeng, Chenzhao Li, Boyang Li, Michael J. Zachman, E.E. Alp, S. Karakalos, Marcos Lucero, Bingzhang Zhang, Maoyu Wang, Zhenxing Feng, Guofeng Wang, Jian Xie, David A. Cullen, Deborah Myers, Jean‐Pol Dodelet, Gang Wu

Bibliographic record

VenueChemRxiv · 2022
Typepreprint
Languageen
FieldEnergy
TopicElectrocatalysts for Energy Conversion
Canadian institutionsInstitut National de la Recherche Scientifique
FundersHydrogen and Fuel Cell Technologies OfficeU.S. Department of Energy
KeywordsCatalysisProton exchange membrane fuel cellThermal stabilityActive siteMembrane electrode assemblyCathodePlatinumChemistryAtmosphere (unit)MetalOxygen reduction reactionChemical engineeringMaterials scienceNanotechnologyElectrodePhysical chemistryElectrochemistryOrganic chemistryThermodynamicsPhysics

Abstract

fetched live from OpenAlex

Fe-N-C catalysts, the most promising platinum group metal (PGM)-free oxygen-reduction catalysts, often simultaneously contain pyrrolic N- (S1) and pyridinic N (S2) -coordinated FeN4 sites. These two types of active sites show significantly different intrinsic activity and stability. S1 sites are more active but less stable compared to S2 sites. Designing a Fe-N-C catalyst, which exclusively contains active S1 sites with enhanced intrinsic stability, is highly desirable to break the activity-stability trade-off. Herein, we report a Fe-N-C model catalyst that solely comprises S1 sites prepared by adding H2 in the pyrolysis atmosphere (i.e., 10% H2/Ar). A membrane electrode assembly (MEA) with the Fe-N-C cathode demonstrated compelling activity and generated a current density of 50.8 mA cm−2 at 0.9 ViR-free (H2-O2) and 211 mA cm−2 at 0.8 V (H2-air), which have significantly exceeded the U.S. DOE 2025 targets. The highly active Fe-N-C catalyst also demonstrated improved stability during life tests and accelerated stability tests (ASTs). The knowledge obtained from experimental and theoretical results elucidates that the FeN4 site formation process can be controlled by thermal activation atmospheres, which is essential to breaking activity-stability trade-off and design viable Fe-N-C catalysts with adequate activity and stability for proton exchange membrane fuel cells.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.014
GPT teacher head0.220
Teacher spread0.206 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations3
Published2022
Admission routes1
Has abstractyes

Explore more

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