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Record W4313340367 · doi:10.1002/adma.202209567

Coordination Polymer Electrocatalysts Enable Efficient CO‐to‐Acetate Conversion

2022· article· en· W4313340367 on OpenAlexafffund
Mingchuan Luo, Adnan Ozden, Ziyun Wang, Fengwang Li, Jianan Erick Huang, Sung‐Fu Hung, Yuhang Wang, Jun Li, Dae‐Hyun Nam, Yuguang Li, Yi Xu, Ruihu Lu, Shuzhen Zhang, Yanwei Lum, Yang Ren, Longlong Fan, Fei Wang, Huihui Li, Dominique Appadoo, Cao‐Thang Dinh, Yuan Liu, Bin Chen, Joshua Wicks, Haijie Chen, David Sinton, Edward H. Sargent

Bibliographic record

VenueAdvanced Materials · 2022
Typearticle
Languageen
FieldEnergy
TopicCO2 Reduction Techniques and Catalysts
Canadian institutionsCanada Research ChairsUniversity of New BrunswickUniversity of Toronto
FundersArgonne National LaboratoryAustralian Research CouncilNatural Sciences and Engineering Research Council of CanadaOffice of ScienceU.S. Department of EnergyAustralian GovernmentCanadian Light SourceMinistry of Science and TechnologyUniversity of Toronto
KeywordsFaraday efficiencyMaterials scienceElectrosynthesisCatalysisChemical engineeringInorganic chemistryElectrochemical reduction of carbon dioxideElectrodeCarbon monoxideElectrochemistryOrganic chemistryChemistry

Abstract

fetched live from OpenAlex

Abstract Upgrading carbon dioxide/monoxide to multi‐carbon C 2+ products using renewable electricity offers one route to more sustainable fuel and chemical production. One of the most appealing products is acetate, the profitable electrosynthesis of which demands a catalyst with higher efficiency. Here, a coordination polymer (CP) catalyst is reported that consists of Cu(I) and benzimidazole units linked via Cu(I)‐imidazole coordination bonds, which enables selective reduction of CO to acetate with a 61% Faradaic efficiency at −0.59 volts versus the reversible hydrogen electrode at a current density of 400 mA cm −2 in flow cells. The catalyst is integrated in a cation exchange membrane‐based membrane electrode assembly that enables stable acetate electrosynthesis for 190 h, while achieving direct collection of concentrated acetate (3.3 molar) from the cathodic liquid stream, an average single‐pass utilization of 50% toward CO‐to‐acetate conversion, and an average acetate full‐cell energy efficiency of 15% at a current density of 250 mA cm −2 .

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.136
Threshold uncertainty score0.998

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0030.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.246
Teacher spread0.239 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations53
Published2022
Admission routes2
Has abstractyes

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