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Record W4319058744 · doi:10.1002/adma.202209685

Versatile Assembly of Metal–Phenolic Network Foams Enabled by Tannin–Cellulose Nanofibers

2023· article· en· W4319058744 on OpenAlexafffund
Bruno D. Mattos, Ya Zhu, Blaise L. Tardy, Marco Beaumont, Ana Carolina Rodrigues Ribeiro, André Luiz Missio, Caio G. Otoni, Orlando J. Rojas

Bibliographic record

VenueAdvanced Materials · 2023
Typearticle
Languageen
FieldEngineering
TopicLignin and Wood Chemistry
Canadian institutionsUniversity of British Columbia
FundersEuropean Research CouncilEuropean CommissionFundação de Amparo à Pesquisa do Estado do Rio Grande do SulCanada Excellence Research Chairs, Government of CanadaFundação de Amparo à Pesquisa do Estado de São PauloCanada Foundation for Innovation
KeywordsMaterials scienceNanofiberCelluloseTanninMetalNanotechnologyPolymer scienceComposite materialChemical engineeringMetallurgy

Abstract

fetched live from OpenAlex

Abstract Metal–phenolic network (MPN) foams are prepared using colloidal suspensions of tannin‐containing cellulose nanofibers (CNFs) that are ice‐templated and thawed in ethanolic media in the presence of metal nitrates. The MPN facilitates the formation of solid foams by air drying, given the strength and self‐supporting nature of the obtained tannin–cellulose nanohybrid structures. The porous characteristics and (dry and wet) compression strength of the foams are rationalized by the development of secondary, cohesive metal‐phenolic layers combined with a hydrogen bonding network involving the CNF. The shrinkage of the MPN foams is as low as 6% for samples prepared with 2.5–10% tannic acid (or condensed tannin at 2.5%) with respect to CNF content. The strength of the MPN foams reaches a maximum at 10% tannic acid (using Fe (III) ions), equivalent to a compressive strength 70% higher than that produced with tannin‐free CNF foams. Overall, a straightforward framework is introduced to synthesize MPN foams whose physical and mechanical properties are tailored by the presence of tannins as well as the metal ion species that enable the metal–phenolic networking. Depending on the metal ion, the foams are amenable to modification according to the desired application.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.052
Threshold uncertainty score0.835

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.207
Teacher spread0.201 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations83
Published2023
Admission routes2
Has abstractyes

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