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Record W4322627756 · doi:10.1002/smsc.202200096

A Strategy to Enhance Humidity Robustness of p‐Type CuO Sensors for Breath Acetone Quantification

2023· article· en· W4322627756 on OpenAlex
Dina N. Oosthuizen, Ines C. Weber

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueSmall Science · 2023
Typearticle
Languageen
FieldEngineering
TopicGas Sensing Nanomaterials and Sensors
Canadian institutionsInstitute of Particle Physics
FundersInnosuisse - Schweizerische Agentur für InnovationsförderungEidgenössische Technische Hochschule ZürichSchweizerischer Nationalfonds zur Förderung der Wissenschaftlichen ForschungNational Science Foundation
KeywordsAcetoneRobustness (evolution)SelectivityX-ray photoelectron spectroscopyRelative humidityNanoclustersHumidityMaterials scienceBreath gas analysisAnalytical Chemistry (journal)Volatile organic compoundChemistryNanotechnologyChemical engineeringChromatographyOrganic chemistry

Abstract

fetched live from OpenAlex

Low‐cost metal oxide sensors are highly attractive for emerging applications such as breath analysis. Particularly promising are p‐type sensors that can operate at low temperatures, a key requirement for compact and low‐power devices. To date, however, these sensors lack sufficient sensitivity, selectivity, and humidity robustness to fulfil stringent requirements faced in real applications. Herein, a flame‐made and low‐power sensor (operated at 150 °C) that consists of CeO 2 ‐decorated CuO nanoparticles is introduced, as determined by X‐ray diffraction and X‐ray photoelectron spectroscopy analysis. Most remarkably, this sensor features excellent robustness to 10–90% relative humidity. This is attributed to the presence of CeO 2 nanoclusters, which may act by scavenging OH − and allow the readsorption of oxygen onto the CuO surface. To demonstrate its immediate impact, this sensor is investigated for the detection of acetone, a biomarker for fat burning. It detects acetone with high sensitivity (i.e., 50 ppb) and features excellent acetone selectivity (>9.8) toward key inorganic interferants (i.e., NH 3 , H 2 , and CO). Most importantly, the CeO 2 –CuO sensor accurately quantifies acetone concentrations in the exhaled breath of 16 volunteers (bias and precision of 90 and 457 ppb). As a result, it is attractive for low‐power and humidity robust detection of volatiles in breath analysis.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.163
Threshold uncertainty score0.379

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.049
GPT teacher head0.298
Teacher spread0.249 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it