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Record W4327564974 · doi:10.1021/acsenergylett.3c00133

Impurity-Resistant CO<sub>2</sub> Reduction Using Reactive Carbon Solutions

2023· article· en· W4327564974 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueACS Energy Letters · 2023
Typearticle
Languageen
FieldEnergy
TopicCO2 Reduction Techniques and Catalysts
Canadian institutionsCanadian Institute for Advanced ResearchUniversity of British Columbia
FundersCanada First Research Excellence FundCanada Foundation for InnovationNatural Sciences and Engineering Research Council of CanadaCanada Research ChairsCanadian Institute for Advanced Research
KeywordsNOxFlue gasChemistryInorganic chemistryDissolutionCarbon fibersImpurityCarbonateRedoxOxidizing agentElectrochemistryCarbon dioxideSulfurOzoneMaterials scienceCombustionElectrodeOrganic chemistry

Abstract

fetched live from OpenAlex

Electrolyzers that electrochemically convert aqueous (bi)carbonate solutions (solutions containing captured CO 2, or “reactive carbon solutions”) into commodity chemicals couple CO 2 capture with CO 2 conversion. Industrial exhaust streams contain nitrogen oxides (NO x ) and sulfur oxides (SO x ) that form redox-active anions in reactive carbon solutions that can interfere with downstream CO 2 reduction. We therefore designed experiments to test how impurities produced from the dissolution of NO x (NO 2 – and NO 3 – ) and SO x (SO 3 2– and SO 4 2– ) impact the electrochemical conversion of (bi)carbonate to CO. We found that CO production was unaffected by SO x compounds in a 3.0 M KHCO 3 feedstock, but 2000 ppm of NO x impurities decreased CO selectivity from ∼60% to <5%. This decrease was caused by the preferential reduction of NO 2 – and NO 3 – over CO 2 . Our study establishes tolerance limits for common flue gas impurities in reactive carbon solutions and provides strategies to mitigate toxification effects.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.012
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.021
GPT teacher head0.247
Teacher spread0.226 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it