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Record W4353036759 · doi:10.1021/acsomega.3c01366

Sour Gas Adsorption on Silica Gels

2023· article· en· W4353036759 on OpenAlexafffund
John H. Jacobs, Kaylan H. McKelvie, Safeer S. Nanji, Robert A. Marriott

Bibliographic record

VenueACS Omega · 2023
Typearticle
Languageen
FieldEngineering
TopicCarbon Dioxide Capture Technologies
Canadian institutionsUniversity of Calgary
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsSilanolAdsorptionHydrogen sulfideBar (unit)MethaneSilica gelChemistryVolume (thermodynamics)Chemical engineeringSilicon dioxideMaterials scienceInorganic chemistryChromatographyOrganic chemistryCatalysisComposite materialThermodynamics

Abstract

fetched live from OpenAlex

High Resolution Image Download MS PowerPoint Slide One of the essential factors for water adsorption on silica gels is the concentration of silanol groups on the silica surface. However, no systematic investigation on the adsorption of sour gas components, methane (CH 4 ), carbon dioxide (CO 2 ), and hydrogen sulfide (H 2 S) on silica gels with different textural properties and surface silanol concentrations, has been conducted. Three silica gels of 22, 30, and 60 Å pore sizes, with silanol concentrations of α total = 2.516, 2.340, and 2.152 OH nm –2, respectively, were studied in this work. The adsorption data for CH 4, CO 2, H 2 S, and H 2 O at T = 0, 25, and 50 °C on the 22 and 30 Å pore size silica gels were presented, and a comparison of the data for the 60 Å pore size silica gel on the same adsorbates was conducted. All three silica gels showed an adsorption affinity in the order of H 2 O > H 2 S > CO 2 > CH 4 . The isosteric heats of adsorption of H 2 O and H 2 S had a greater dependence on the silanol concentration than CO 2 and CH 4 . At p < 10 bar, there was no difference in the adsorption per m 2 of CH 4 between the silica gels ( n ads = 1.7 mmol m –2, for all silicas at p = 10 bar), while higher pressures resulted in greater adsorption capacity in the larger pore volume silica gels (at p = 20 bar: n ads = 3.0, 3.3, and 3.4 mmol m –2 for the 22, 30, and 60 Å pore size silicas, respectively). H 2 S adsorption at low pressures ( p < 4 bar) was larger on the samples with larger silanol concentrations (at p = 3 bar: n ads = 6.1, 4.7, and 4.5 mmol m –2 for the 22, 30, and 60 Å pore size silicas, respectively), but above p = 4 bar, the 60 Å pore size silica had a greater adsorption capacity than the 30 Å pore size (at p = 5 bar: n ads = 8.0, 6.0, and 6.2 mmol m –2 for the 22, 30, and 60 Å pore size silicas, respectively).

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.123
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.014
GPT teacher head0.215
Teacher spread0.202 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations11
Published2023
Admission routes2
Has abstractyes

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