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Record W4376107457 · doi:10.1021/acsaem.3c00613

Transition-Metal and Nitrogen-Doped Carbon Nanotube/Graphene Composites as Cathode Catalysts for Anion-Exchange Membrane Fuel Cells

2023· article· en· W4376107457 on OpenAlexaff
Jaana Lilloja, Elo Kibena‐Põldsepp, Ave Sarapuu, Anastasiia Konovalova, Maike Käärik, Jekaterina Kozlova, Päärn Paiste, Arvo Kikas, Alexey Treshchalov, Jaan Aruväli, Andrea Zitolo, Jaan Leis, Aile Tamm, Vambola Kisand, Steven Holdcroft, Kaido Tammeveski

Bibliographic record

VenueACS Applied Energy Materials · 2023
Typearticle
Languageen
FieldEnergy
TopicElectrocatalysts for Energy Conversion
Canadian institutionsSimon Fraser University
FundersEuropean Regional Development FundEesti Teadusagentuur
KeywordsCatalysisMaterials scienceCarbon nanotubeGrapheneTransition metalCobaltCarbon fibersChemical engineeringElectrochemistryPyrolysisCathodeNanoparticleInorganic chemistryComposite materialNanotechnologyElectrodeChemistryOrganic chemistryPhysical chemistryComposite numberMetallurgy

Abstract

fetched live from OpenAlex

Transition-metal and nitrogen-doped graphene-like material and carbon nanotube (M-N-Gra/CNT) composites are prepared, characterized, and used as cathode catalysts in anion-exchange membrane fuel cells (AEMFCs). Melamine as a nitrogen source and cheap iron and cobalt salts as metal precursors are used for doping via high-temperature pyrolysis. The success of doping is proven by several physicochemical analysis methods, and the catalyst materials possess rather similar textural properties. The initial assessment of the oxygen reduction reaction activity using the rotating disk electrode method shows that Fe-N-Gra/CNT, Co-N-Gra/CNT, and CoFe-N-Gra/CNT materials have very similar electrocatalytic performances in alkaline media as well as excellent short-term stability but a different yield of HO 2 – formation. The M-N-Gra/CNT materials as cathode catalysts together with the Aemion+ reinforced anion-exchange membrane exhibit very good AEMFC performance, especially CoFe-N-Gra/CNT, comparable to that of Pt/C, reaching a peak power density of 638 mW cm –2 . Such an excellent fuel cell performance of the M-N-Gra/CNT catalyst materials is attributed to the presence of M–N x sites, carbon-encapsulated transition-metal nanoparticles, and feasible nitrogen-containing moieties.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0010.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.211
Teacher spread0.203 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations23
Published2023
Admission routes1
Has abstractyes

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