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Record W4380885814 · doi:10.26434/chemrxiv-2023-hng1x

Amorphous 1-D nanowires of calcium phosphate/pyrophosphate: a demonstration of orientated growth of amorphous minerals

2023· preprint· en· W4380885814 on OpenAlexaff
Chaobo Feng, Bing‐Qiang Lu, Yunshan Fan, Haijian Ni, Yunfei Zhao, Shuo Tan, Zhi Zhou, Lijia Liu, Jordan A. Hachtel, Demie Kepaptsoglou, Denis Gebauer, Shisheng He, Feng Chen

Bibliographic record

VenueChemRxiv · 2023
Typepreprint
Languageen
FieldMaterials Science
TopicCalcium Carbonate Crystallization and Inhibition
Canadian institutionsWestern University
FundersOak Ridge National LaboratoryEngineering and Physical Sciences Research CouncilOffice of ScienceEast China Normal UniversityNational Natural Science Foundation of ChinaUT-BattelleLaboratory Directed Research and DevelopmentU.S. Department of EnergyScience and Technology Commission of Shanghai MunicipalityBattelle
KeywordsAmorphous solidAmorphous calcium phosphatePyrophosphateMaterials scienceChemical engineeringNanotechnologyBiomineralizationNanoclustersNanoparticleMineralogyCalciumCrystallographyChemistryMetallurgyOrganic chemistry

Abstract

fetched live from OpenAlex

Amorphous inorganic solids are traditionally isotropic, thus, it is believed that they only grow into morphologies of nanospheres or irregular aggregates of nanoparticles. However, in the presence of (ortho)phosphate (Pi) and pyrophosphate ions (PPi) which have synergistic roles in biomineralization, amorphous calcium phosphate-pyrophosphate nanowires (ACPPNs) form in an aqueous additive-free solution. Cryo-TEM shows that the single nanowire has an average diameter of 2-3 nm, and lengths of up to hundreds of nanometers. In ACPPNs, amorphous calcium orthophosphate and amorphous calcium pyrophosphate are distributed at separated but close sites. The ACPPNs grow via either the preferential attachment of ~2 nm nanoclusters in 1-dimension way, or the transformation of bigger nanoparticles. We propose that the anisotropy of ACPPNs microstructure, which is corroborated experimentally, causes their oriented growth. This study proves that, unlike the conventional view, amorphous minerals can form via oriented growth without external regulation, demonstrating a novel insights into the structures and growth behaviors of amorphous minerals.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.001
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.035
GPT teacher head0.269
Teacher spread0.234 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2023
Admission routes1
Has abstractyes

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