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Record W4384131691 · doi:10.1002/cjce.25040

The development of a novel non‐leaching flocculant, derived from activated carbon and polyacrylamide

2023· article· en· W4384131691 on OpenAlexaffvenueabout
Kevin M. Scotland, Sarah Bégin, Oliver K.L. Strong, Paul R. Pede, Andrew J. Vreugdenhil

Bibliographic record

VenueThe Canadian Journal of Chemical Engineering · 2023
Typearticle
Languageen
FieldEngineering
TopicEnhanced Oil Recovery Techniques
Canadian institutionsCarbon Engineering (Canada)Trent University
Fundersnot available
KeywordsPolyacrylamideFlocculationChemical engineeringLeaching (pedology)PolymerDewateringChemistryTailingsSettlingDivinylbenzeneDemulsifierMaterials sciencePulp and paper industryWaste managementStyreneCopolymerEnvironmental engineeringPolymer chemistryOrganic chemistryEnvironmental scienceMetallurgyEmulsion

Abstract

fetched live from OpenAlex

Abstract Canadian oil sands are the third largest oil reserves in the world, containing an estimated 28.3 billion m 3 of recoverable bitumen. Extraction of bitumen via surface mining and water‐based extraction leads to the formation of tailings ponds, which contain slow settling mature fine tailings (MFT). These MFT can take hundreds of years to settle on their own. Polymer flocculants are used to improve the settling rate of the MFT. This requires a significant amount of polymer, which may itself have environmental impacts. Here, we describe development of a solid‐state flocculant using activated carbon (AC) as a backbone for polyacrylamide (PAM) flocculant branches, with the intention that this solid‐state flocculant would reduce the amount of polymer applied, replacing the bulk of the material with hydrophobic AC, and limit leaching of these materials. The development of this flocculant is achieved by bromination of AC followed by reaction with cis ‐octadecen‐1‐ol at the carbon surface. Subsequently, PAM was attached to the alkene of the enol via thermally induced radical polymerization. This AC‐PAM demonstrated effective flocculation of 5% MFTs at a minimum dosage of 120,000 ppm with an initial settling rate of 33 m/h. Thermogravimetric analysis determined that the AC‐PAM had 2% PAM content, indicating that the system only uses 2400 ppm polymer, which is a significant reduction when compared to the typical 20,000 ppm of PAM otherwise required to flocculate 5% MFTs. This demonstrates a marked reduction in the polymer required to flocculate MFTs, reducing potential environment impact.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.000
Threshold uncertainty score0.001

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.195
Teacher spread0.186 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations3
Published2023
Admission routes3
Has abstractyes

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