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Record W4385543422 · doi:10.3390/en16155781

Reverse Water Gas Shift versus Carbon Dioxide Electro-Reduction: The Reaction Pathway Responsible for Carbon Monoxide Production in Solid Oxide Co-Electrolysis Cells

2023· article· en· W4385543422 on OpenAlexaff
Anders S. Nielsen, Brant A. Peppley, Odne Stokke Burheim

Bibliographic record

VenueEnergies · 2023
Typearticle
Languageen
FieldMaterials Science
TopicAdvancements in Solid Oxide Fuel Cells
Canadian institutionsQueen's University
FundersEnersense, Norway
KeywordsElectrolysisCarbon monoxideWater-gas shift reactionChemistryElectrolysis of waterChemical engineeringPolymer electrolyte membrane electrolysisSteam reformingHigh-temperature electrolysisHydrogen productionInorganic chemistryCarbon dioxideElectrochemical reduction of carbon dioxideOxidePolarization (electrochemistry)HydrogenCatalysisOrganic chemistryElectrodePhysical chemistry

Abstract

fetched live from OpenAlex

Solid oxide co-electrolysis cells can utilize renewable energy sources for the conversion of steam and carbon dioxide into valuable chemicals and feedstocks. An important challenge in the analysis of these devices is understanding the reaction pathway(s) that govern carbon monoxide generation. Studies in which co-electrolysis polarization lies between those of pure steam and pure carbon dioxide electrolysis suggest that carbon dioxide electro-reduction (CO2ER) and the reverse water gas shift (RWGS) reaction are both contributors to CO generation. However, experiments in which co-electrolysis polarization overlaps that of pure steam electrolysis propose that the RWGS reaction dominates CO production and CO2ER is negligible. Supported by dimensional analysis, thermodynamics, and reaction kinetics, this work elucidates the reasons for which the latter conclusion is infeasible, and provides evidence for why the observed overlap between co-electrolysis and pure steam electrolysis is a result of the slow kinetics of CO2ER in comparison to that of steam, with the RWGS reaction being inconsequential. For sufficiently thin cathode current collectors, we reveal that CO2ER is dominant over the RWGS reaction, while the rate of steam electro-reduction is much higher than that of carbon dioxide, which causes the co-electrolysis and pure steam electrolysis polarization curves to overlap. This is contrary to what has been proposed in previous experimental analyses. Ultimately, this work provides insight into how to design solid oxide co-electrolysis cells such that they can exploit a desired reaction pathway in order to improve their efficiency and product selectivity.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0010.001
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.019
GPT teacher head0.278
Teacher spread0.258 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations6
Published2023
Admission routes1
Has abstractyes

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