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Record W4385638294 · doi:10.1021/acsenergylett.3c01157

Rapidly In Situ Cross-Linked Poly(butylene oxide) Electrolyte Interface Enabling Halide-Based All-Solid-State Lithium Metal Batteries

2023· article· en· W4385638294 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueACS Energy Letters · 2023
Typearticle
Languageen
FieldEngineering
TopicAdvanced Battery Materials and Technologies
Canadian institutionsWestern University
FundersNatural Sciences and Engineering Research Council of CanadaMitacsCanada Research ChairsGLABAT Solid-State BatteryChina Automotive Battery Research InstituteWestern UniversityCanada Foundation for InnovationOntario Research FoundationCanadian Light Source
KeywordsElectrolyteHalideAnodeMaterials scienceOxideCathodeLithium (medication)Chemical engineeringLithium metalInorganic chemistryQuasi-solidMetalFast ion conductorElectrodeChemistryPhysical chemistryMetallurgy

Abstract

fetched live from OpenAlex

Halide-based solid-state halide electrolytes (SSEs) were recently revived as promising candidates for next-generation all-solid-state batteries due to their superionic conductivity, direct compatibility with high-voltage cathodes, and scalable production. However, the incompatibility between halide SSEs and lithium metal anodes remains a main challenge to achieve high energy density. Herein, we demonstrate a thin cross-linked poly(butylene oxide) solid polymer electrolyte (xPBO SPE) interlayer on the superionic Li 3 InCl 6 SSE to enable lithium metal compatibility. A rapid and solvent-free in situ cross-linking process is developed by reaction between a 0.5 s pulse of trimethylaluminum vapor and the hydroxyl terminal groups of poly(butylene oxide). The Li–Li symmetric cells using xPBO-SPE@Li 3 InCl 6 demonstrate a highly stable cycling performance over 1100 h and up to 1.0 mA cm –2 and 1.0 mAh cm –2 . All-solid-state lithium metal battery (ASSLMB) performance with a LiCoO 2 cathode is presented. This new rapid cross-linking strategy shall inspire more possibilities for lithium metal anode integration in ASSLMBs.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.156
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.011
GPT teacher head0.247
Teacher spread0.236 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it