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Record W4385727195 · doi:10.1021/acssuschemeng.3c03492

Various-Sized Nanocelluloses Induced Stereocomplexes Crystallization Formation and Its Mechanism of Stereoisomers Poly(lactide acid) Blend

2023· article· en· W4385727195 on OpenAlexaff
Yao Xie, Somia Yassin Hussain Abdalkarim, Ze Sheng Ji, Zhiming Chen, Mingxin Wang, Hou–Yong Yu

Bibliographic record

VenueACS Sustainable Chemistry & Engineering · 2023
Typearticle
Languageen
FieldMaterials Science
TopicAdvanced Cellulose Research Studies
Canadian institutionsUniversity of Waterloo
FundersPrimary Research and Development Plan of Zhejiang ProvinceZhejiang Sci-Tech UniversityNatural Science Foundation of Zhejiang ProvinceNational Natural Science Foundation of China
KeywordsNanocompositeMaterials scienceCrystallizationChemical engineeringNucleationCrystallinityUltimate tensile strengthCelluloseHydrogen bondPolymerComposite materialPolymer chemistryOrganic chemistryChemistryMolecule

Abstract

fetched live from OpenAlex

This work provides evidence to explore the relationship between hydrogen bonding interactions and stereocomplex crystallization (SC) formation of nanocomposite-based nanocelluloses (NCs). Here, we evaluated the synergistic effect of various aspect ratios of NCs as nucleating agents on the properties of a poly( l -lactic acid)/poly( d -lactic acid) ( l / d ) stereocomplexable matrix using the casting method. Furthermore, NCs enhanced the interfacial adhesion interaction of the l / d matrix, improving crystallization ability, heat resistance, and barrier properties against the water vapor of nanocomposites. As expected, the nanocomposite with cellulose nanofibers (CNF 3 ) had the highest SC crystallinity of 33.9% and a maximum SC melting temperature of 220.6 °C. The tensile strength of the l / d /CNF 3 nanocomposite increased to 53.0 MPa due to the highest aspect ratio and rigidity of CNF, which improved interfacial hydrogen bonding interactions between CNF 3 and the l / d matrix. Compared with different samples, nanocomposite with cellulose nanospheres (CNS 3 ) had the smallest spherulite size. While nanocomposite with cellulose nanocrystals (CNC 3 ) exhibited more efficient heterogeneous nucleation than that of CNS 3 or CNF 3 . We demonstrated the relationship between the hydrogen-bonding interactions of l / d nanocomposites and crystallization kinetic/mechanism. This work offers a suitable strategy for selecting appropriate types of NCs as nucleating agents for designing high-performance materials for food packaging industries to solve the plastic melt processing problem.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.009
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.015
GPT teacher head0.242
Teacher spread0.227 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations23
Published2023
Admission routes1
Has abstractyes

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