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Record W4386255599 · doi:10.26434/chemrxiv-2023-8dxvc

General rules for the design of molecular photoswitches based on electrocyclization

2023· preprint· en· W4386255599 on OpenAlexafffund
Clàudia Climent, Zhen Xu, Michael O. Wolf, David Casanova

Bibliographic record

VenueChemRxiv · 2023
Typepreprint
Languageen
FieldMaterials Science
TopicPhotochromic and Fluorescence Chemistry
Canadian institutionsUniversity of British Columbia
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsMolecular orbitalRing (chemistry)Molecular switchMoleculeComputational chemistryAromaticityChromophoreChemistrySimple (philosophy)Chemical physicsPhotochromismAtomic orbitalNanotechnologyMaterials sciencePhysicsPhotochemistryQuantum mechanicsOrganic chemistry

Abstract

fetched live from OpenAlex

Molecular photoswitches undergo a structural transformation upon excitation with light to intraconvert between two or more stable forms. In some cases, the structural rearrangement involves a cyclization reaction, that is, the transition between ring-open and ring-closed molecular forms. In this work we develop simple guidelines for the design of organic molecules able to undergo photochemical electrocyclization, using electronic structure calculations on one of the most widely-used family of molecules in the field, dithienylethene (DTE)-based compounds. We conclude that the ability to photocyclize can be predicted from the localization and symmetry of frontier molecular orbitals. These ideas are based on the Woodward- Hoffmann rules, but go beyond them, allowing the behavior of a more general family of chromophores, chemically substituted DTEs, to be understood. Moreover, our rules have been validated by assessment of a large number of molecular photoswitches that have been previously investigated experimentally. We have also explored the relationship between thermal stability of the closed form and aromaticity. We use the DTE scaffold as the workhorse model in our computational study, however, these simple yet powerful guidelines are expected to be generally valid to guide the design of other diarylethenes.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.371
Threshold uncertainty score0.713

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.040
GPT teacher head0.269
Teacher spread0.230 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2023
Admission routes2
Has abstractyes

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