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Record W4386700073 · doi:10.1149/1945-7111/acf95e

Studying The Impact of Electrolyte, Li Excess, NMC Blending, and Cycling Conditions on The Lifetime and Degradation of LMO/AG Cells Using UHPC Cycling, XRF, and Isothermal Microcalorimetry

2023· article· en· W4386700073 on OpenAlexaff
Ahmed Eldesoky, Nicole Kowalski, Haoqi Ni, E. R. Logan, Eniko Zsoldos, Animesh Dutta, Nian Zhang, J. R. Dahn

Bibliographic record

VenueJournal of The Electrochemical Society · 2023
Typearticle
Languageen
FieldEngineering
TopicAdvancements in Battery Materials
Canadian institutionsDalhousie University
Fundersnot available
KeywordsIsothermal microcalorimetryElectrolyteCoulometryIsothermal processCyclingElectrodeDegradation (telecommunications)Materials scienceTemperature cyclingAnalytical Chemistry (journal)Chemical engineeringElectrochemistryChemistryInorganic chemistryThermodynamicsChromatographyPhysical chemistry

Abstract

fetched live from OpenAlex

The impact of electrolyte, Li excess, NMC blending, and cycling conditions on the performance of Li 1+x Mn 2-x O 4 (LMO)/Artificial Graphite (AG) cells was studied using ultra-high precision coulometry (UHPC), X-ray fluorescence (XRF), and isothermal microcalorimetry (IMC). Decreasing the Li excess resulted in severe capacity fade which was greatly improved by blending LMO with NMC622. The known synergy between NMC and LMO is electrolyte-dependant and was more significant at elevated temperatures. We showed with XRF that Mn deposition on the negative electrode occurs primarily during the early cycles and is reduced by increasing the Li excess in LMO or by blending with NMC622. IMC experiments demonstrates a correlation between parasitic heat flow and Mn loading on the negative electrode and gas generation. Finally, LiFSI co-salts were examined to suppress Al corrosion while retaining the beneficial role of LiFSI in improving cell performance.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.004

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.016
GPT teacher head0.278
Teacher spread0.262 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations18
Published2023
Admission routes1
Has abstractyes

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Same venueJournal of The Electrochemical SocietySame topicAdvancements in Battery MaterialsFrench-language works237,207