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Record W4386714095 · doi:10.1002/cjce.25076

Deep chemometrics using one‐dimensional convolutional neural networks for predicting crude oil properties from FTIR spectral data

2023· article· en· W4386714095 on OpenAlexafffundvenue
Souvik Ta, Shahla Alizadeh, S. Lakshminarayanan, Ajay K. Ray

Bibliographic record

VenueThe Canadian Journal of Chemical Engineering · 2023
Typearticle
Languageen
FieldChemistry
TopicSpectroscopy and Chemometric Analyses
Canadian institutionsWestern University
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsPartial least squares regressionChemometricsConvolutional neural networkInterpretabilityBiological systemArtificial neural networkPrincipal component analysisFourier transform infrared spectroscopyComputer scienceArtificial intelligencePrincipal component regressionPattern recognition (psychology)Fourier transformPreprocessorMean squared errorMathematicsStatisticsMachine learningOpticsPhysics

Abstract

fetched live from OpenAlex

Abstract The determination of physicochemical properties of crude oils is a very important and time‐intensive process that needs elaborate laboratory procedures. Over the last few decades, several correlations have been developed to estimate these properties, but they have been very limited in their scope and range. In recent years, methods based on spectral data analysis have been shown to be very promising in characterizing petroleum crude. In this work, the physicochemical properties of crude oils using Fourier transform infrared (FTIR) spectrums are predicted. A total of 107 samples of FTIR spectral data consisting of 6840 wavenumbers is used. One dimensional convolutional neural networks (CNNs) were used employing FTIR spectral data as the one‐dimensional input and Keras and TensorFlow were used for model building. The Root Mean Square Error decreased from 160 to around 60 for viscosity when compared to previous machine learning methods like partial least squares (PLS), principal component regression (PCR), and partial least squares regression with genetic algorithm (PLS‐GA) on the same data. The important hyper‐parameters of the CNN were optimized. In addition, a comparison of results obtained with different neural network architectures is presented. Some common preprocessing techniques were also tested on the spectral data to determine their impact on model performance. To increase interpretability, the intermediate neural network layers were analyzed to reveal what the convolutions represented, and sensitivity analysis was done to gather key insights about the wavenumbers that were the most important for prediction of the crude oil properties using the neural network.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Simulation or modeling · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.471
Threshold uncertainty score0.702

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.055
GPT teacher head0.243
Teacher spread0.187 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designSimulation or modeling
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations6
Published2023
Admission routes3
Has abstractyes

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