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Record W4386878501 · doi:10.1021/acsinfecdis.3c00203

Discovery of a Druggable, Cryptic Pocket in SARS-CoV-2 nsp16 Using Allosteric Inhibitors

2023· article· en· W4386878501 on OpenAlexafffund
Nicole L. Inniss, Ján Kozic, Fengling Li, Mónica Rosas‐Lemus, G. Minasov, Jiří Rybáček, Yingjie Zhu, Radek Pohl, L. Shuvalova, Lubomı́r Rulı́šek, J.S. Brunzelle, Lucie Bednářová, Milan Štefek, Ján Michael Kormaník, Erik Andris, Jaroslav Šebestı́k, Alice Shi Ming Li, Peter J. Brown, Uli Schmitz, Kumar Singh Saikatendu, Edcon Chang, Radim Nencka, Masoud Vedadi, K.J.F. Satchell

Bibliographic record

VenueACS Infectious Diseases · 2023
Typearticle
Languageen
FieldMedicine
TopicSARS-CoV-2 and COVID-19 Research
Canadian institutionsStructural Genomics ConsortiumOntario Institute for Cancer ResearchUniversity of Toronto
FundersNational Institute of Allergy and Infectious DiseasesArgonne National LaboratoryOntario Genomics InstituteNational Institute of General Medical SciencesGenome CanadaMichigan Technology Tri-CorridorAkademie Věd České RepublikyOffice of ScienceMinisterstvo Zdravotnictví Ceské RepublikyGenentechBristol-Myers SquibbGovernment of OntarioBayerNational Cancer InstituteEuropean Federation of Pharmaceutical Industries and AssociationsEuropean Regional Development FundMerck KGaANational Institutes of HealthTakeda Pharmaceuticals InternationalU.S. Department of Health and Human ServicesOntario GenomicsPfizerNorthwestern UniversityMcGill UniversityU.S. Department of Energy
KeywordsDruggabilityDrug discoveryAllosteric regulationSmall moleculeCoronavirusVirtual screeningBiologyComputational biologySevere acute respiratory syndrome coronavirus 2 (SARS-CoV-2)Binding siteLigand (biochemistry)VirologyChemistryStereochemistryBiochemistryEnzymeCoronavirus disease 2019 (COVID-19)Medicine

Abstract

fetched live from OpenAlex

A collaborative, open-science team undertook discovery of novel small molecule inhibitors of the SARS-CoV-2 nsp16-nsp10 2′- O -methyltransferase using a high throughput screening approach with the potential to reveal new inhibition strategies. This screen yielded compound 5a, a ligand possessing an electron-deficient double bond, as an inhibitor of SARS-CoV-2 nsp16 activity. Surprisingly, X-ray crystal structures revealed that 5a covalently binds within a previously unrecognized cryptic pocket near the S -adenosylmethionine binding cleft in a manner that prevents occupation by S -adenosylmethionine. Using a multidisciplinary approach, we examined the mechanism of binding of compound 5a to the nsp16 cryptic pocket and developed 5a derivatives that inhibited nsp16 activity and murine hepatitis virus replication in rat lung epithelial cells but proved cytotoxic to cell lines canonically used to examine SARS-CoV-2 infection. Our study reveals the druggability of this newly discovered SARS-CoV-2 nsp16 cryptic pocket, provides novel tool compounds to explore the site, and suggests a new approach for discovery of nsp16 inhibition-based pan-coronavirus therapeutics through structure-guided drug design.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.005

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.042
GPT teacher head0.350
Teacher spread0.308 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations22
Published2023
Admission routes2
Has abstractyes

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