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Record W4387266487 · doi:10.1021/acscatal.3c01897

Fluorine-Stabilized BO<sub>6</sub> Octahedron of Host Perovskites for Robust Carbon Dioxide Electrolysis on Exsolved Catalysts

2023· article· en· W4387266487 on OpenAlexafffund
Bowen Zhang, Mengnan Zhu, Min‐Rui Gao, Xiaoyu Liu, Jing Shen, Xiuan Xi, Nanqi Duan, Natalia Semagina, Hongbo Zeng, Jing‐Li Luo

Bibliographic record

VenueACS Catalysis · 2023
Typearticle
Languageen
FieldMaterials Science
TopicAdvancements in Solid Oxide Fuel Cells
Canadian institutionsUniversity of Alberta
FundersNatural Sciences and Engineering Research Council of CanadaCanada First Research Excellence FundUniversity of AlbertaAlberta Innovates - Technology Futures
KeywordsPerovskite (structure)ElectrolysisMaterials scienceCatalysisElectrocatalystOxideOxygen evolutionInorganic chemistryOctahedronFluorineChemical engineeringChemistryElectrodePhysical chemistryCrystal structureElectrochemistryCrystallographyElectrolyteMetallurgy

Abstract

fetched live from OpenAlex

Exsolution of nanoparticles has become a prevalent technique for enhancing the catalytic activity of perovskites for carbon dioxide (CO 2 ) electrolysis in solid oxide electrolysis cells. However, the potential negative impact of phase evolution of the host perovskite on catalytic performance is often overlooked in light of the overall performance enhancement from exsolution. Herein, we illustrate a facile fluorine doping strategy to suppress the phase transition of Sr 2 Fe 1.2 Ni 0.3 Mo 0.5 O 6 –δ (SFN 3 M) during exsolution. The experimental characterizations combined with density functional theory calculations reveal that the incorporation of fluorine into the SFN 3 M lattice is beneficial for preserving the high oxidation states of B-site cations and inhibiting the lattice oxygen loss, resulting in a robust BO 6 octahedron in the host perovskite. It is found that the well-preserved double perovskite structure exhibits a stronger interaction with CO 2, thus enhancing the catalytic activity of F-doped exsolved SFN 3 M (F-SFN 3 M-red). Furthermore, the robust BO 6 octahedron of the host perovskite significantly enhances the resistance of F-SFN 3 M-red to decomposition under high-voltage CO 2 electrolysis, leading to the significantly increased carbon monoxide productivity over a broad voltage range. These findings highlight that the F doping strategy has great potential to aid the development of exsolved perovskites with high catalytic activity and stability for a wider range of electrocatalysis applications.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0010.002
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.018
GPT teacher head0.255
Teacher spread0.237 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations20
Published2023
Admission routes2
Has abstractyes

Explore more

Same venueACS CatalysisSame topicAdvancements in Solid Oxide Fuel CellsFrench-language works237,207