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Record W4387721248 · doi:10.1016/j.mineng.2023.108447

Synergistic, extractive, and selective separation of light, medium, and heavy rare earth elements using Cyanex 572 and Alamine 336 from a chloride medium

2023· article· en· W4387721248 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueMinerals Engineering · 2023
Typearticle
Languageen
FieldEngineering
TopicExtraction and Separation Processes
Canadian institutionsQueen's University
FundersUniversity of TehranQueen's University
KeywordsExtraction (chemistry)ChemistryChlorideCationic polymerizationFourier transform infrared spectroscopyNuclear chemistryChemical engineeringChromatographyOrganic chemistry

Abstract

fetched live from OpenAlex

In this study, the solvent extraction of rare earth elements (REEs) of different groups of light (LREE), medium (MREE), and heavy (HREE) from a chloride medium using the mixture of Cyanex 572 (cationic extractant, organophosphorus-based) and Alamine 336 (anionic extractant, amine-based) was studied. The results showed higher extraction efficiency for HREEs when sole Cyanex 572 was used. However, the addition of Alamine 336 to Cyanex 572 increased the extraction efficiency of LREEs and MREEs. The optimal volumetric ratio of Alamine 336 to Cyanex 572 for maximum extraction efficiency, under the studied conditions, was concluded to be 1:1 at a total extractant concentration of 30 % v/v. The synergistic enhancement factor when using this system for the extraction of LREEs and MREEs varied from 2 to 76 at different pH values and Alamine 336 ratios. To analyze the synergistic effect of the addition of Alamine 336 to Cyanex 572 on REE extraction, slope analysis and Fourier transform infrared spectroscopy measurement were performed. It was concluded that the role of Alamine 336 could be that of a proton ion extractor (released from the Cyanex 572 structure during REEs extraction) for REECl 2+ complexes and that of a phase modifier for Cyanex 572 for REECl 2 + complexes.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.372
Threshold uncertainty score0.939

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.015
GPT teacher head0.255
Teacher spread0.240 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it