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Record W4387931950 · doi:10.1002/smll.202305769

Transport Properties and Local Ions Dynamics in LATP‐Based Hybrid Solid Electrolytes

2023· article· en· W4387931950 on OpenAlexaff
Nicola Boaretto, Pedram Ghorbanzade, Haritz Pérez-Furundarena, Leire Meabe, Juan Miguel López del Amo, Isuru E. Gunathilaka, Maria Forsyth, Jörg Schuhmacher, Andreas Roters, Sergey Krachkovskiy, Abdelbast Guerfi, Michel Armand, María Martínez‐Ibáñez

Bibliographic record

VenueSmall · 2023
Typearticle
Languageen
FieldEngineering
TopicAdvanced Battery Materials and Technologies
Canadian institutionsHydro-Québec
FundersH2020 Marie Skłodowska-Curie ActionsEuropean Commission
KeywordsElectrolyteDielectric spectroscopyConductivityIonic conductivityMaterials scienceIonic bondingPulsed field gradientElectrochemistryChemical physicsAnalytical Chemistry (journal)IonDiffusionChemistryPhysical chemistryThermodynamicsElectrodeOrganic chemistry

Abstract

fetched live from OpenAlex

Abstract Hybrid solid electrolytes (HSEs), namely mixtures of polymer and inorganic electrolytes, have supposedly improved properties with respect to inorganic and polymer electrolytes. In practice, HSEs often show ionic conductivity below expectations, as the high interface resistance limits the contribution of inorganic electrolyte particles to the charge transport process. In this study, the transport properties of a series of HSEs containing Li (1+ x ) Al x Ti (2– x ) (PO 4 ) 3 (LATP) as Li + ‐conducting filler are analyzed. The occurrence of Li + exchange across the two phases is proved by isotope exchange experiment, coupled with 6 Li/ 7 Li nuclear magnetic resonance (NMR), and by 2D 6 Li exchange spectroscopy (EXSY), which gives a time constant for Li + exchange of about 50 ms at 60 °C. Electrochemical impedance spectroscopy (EIS) distinguishes a short‐range and a long‐range conductivity, the latter decreasing with LATP concentration. LATP particles contribute to the overall conductivity only at high temperatures and at high LATP concentrations. Pulsed field gradient (PFG)‐NMR suggests a selective decrease of the anions’ diffusivity at high temperatures, translating into a marginal increase of the Li + transference number. Although the transport properties are only marginally affected, addition of moderate amounts of LATP to polymer electrolytes enhances their mechanical properties, thus improving the plating/stripping performance and processability.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Simulation or modeling · Consensus signal: Simulation or modeling
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.115
Threshold uncertainty score0.322

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.016
GPT teacher head0.194
Teacher spread0.177 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designSimulation or modeling
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations26
Published2023
Admission routes1
Has abstractyes

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