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Record W4388128916 · doi:10.1021/acs.iecr.3c02910

Hierarchical Porous MOF-199 and Zeolite Composites with High Adsorption Performance for Both Toluene and Acetone

2023· article· en· W4388128916 on OpenAlexaff
Xiaomi Meng, Zhongde Dai, Charles Q. Jia, Lin Yang, Wenju Jiang, Lu Yao, Qiying Zhou, Bo Xu

Bibliographic record

VenueIndustrial & Engineering Chemistry Research · 2023
Typearticle
Languageen
FieldChemistry
TopicMetal-Organic Frameworks: Synthesis and Applications
Canadian institutionsUniversity of Toronto
FundersNational Key Research and Development Program of ChinaPostdoctoral Research Foundation of ChinaNatural Science Foundation of Sichuan Province
KeywordsTolueneAdsorptionAcetoneMesoporous materialZeoliteDesorptionChemical engineeringMaterials sciencePorosityMetal-organic frameworkChemistrySpecific surface areaOrganic chemistryCatalysisComposite material

Abstract

fetched live from OpenAlex

In this study, FAU LSP ( n )/MOF-199 composites with hierarchical porous structures have been synthesized by zeolite-induced in situ growth of MOF-199 and applied for efficient adsorption of toluene and acetone. The results revealed that the presence of FAU LSP triggered morphology evolution and developed new structural defects of MOF-199 due to the coordination of FAU LSP and the linker, resulting in a hierarchical porous structure of FAU LSP ( n )/MOF-199. The S BET of FAU LSP ( n )/MOF-199 ranged from 1013 to 1344 cm 2 g –1, comparable to or even superior to that of MOF-199 (1035 cm 2 g –1 ). FAU LSP ( n )/MOF-199 had more developed mesoporous structures ( V mes ), increased from 0.027 cm 3 g –1 of MOF-199 to 0.354 cm 3 g –1 of FAU LSP (15)/MOF-199. The integrated surface chemistry coupled with the derived hierarchical porous structure provided FAU LSP ( n )/MOF-199 a good adsorption property of both weakly polar toluene and strongly polar acetone. The FAU LSP (4)/MOF-199 showed the best adsorption performance with saturated adsorption capacities of 430.2 and 311.1 mg g –1 of toluene and acetone at 25 °C and 1000 mg m –3 . The FAU LSP ( n )/MOF-199 also exhibited excellent adsorption–desorption stability, with only 4.55 and 8.05% capacity loss of toluene and acetone after five adsorption–desorption cycles. According to the characterization before and after adsorption, the kinetic and thermodynamic studies knew that the adsorption of toluene and acetone on FAU LSP ( n )/MOF-199 was mostly a physical-adsorption process, in which both monolayer and multilayer adsorption coexisted.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.048
GPT teacher head0.290
Teacher spread0.242 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations14
Published2023
Admission routes1
Has abstractyes

Explore more

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