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Record W4389205988 · doi:10.22215/etd/2021-15757

Synthesis and Characterization of Oil Lubricant Antioxidant Degradation Products

2021· dissertation· en· W4389205988 on OpenAlexaff
John Rivada

Bibliographic record

Venuenot available
Typedissertation
Languageen
FieldEngineering
TopicLubricants and Their Additives
Canadian institutionsCarleton University
Fundersnot available
KeywordsLubricantAntioxidantDegradation (telecommunications)Organic chemistryChemistryDimerRaw materialPolymer chemistry

Abstract

fetched live from OpenAlex

Antioxidants are an example of additives added to lubricants as a sacrificial substance, which extend the lifespan by preferentially being oxidized over the lubricant. GasTops Ltd. is interested in predicting the remaining life of a lubricant by monitoring the quantity of antioxidant degradation products. An antioxidants of interest is N-phenyl-1-aminonaphthalene (PAN). Three major oxidation products of PAN have been identified, synthesized, and isolated: C-C coupled PAN dimer, C-N coupled PAN dimer, and naphthyl oxidized PAN (Fremy’s PAN). Other products include N-O radical PAN and phenyl oxidized PAN. Attempts to independently synthesize samples of these PAN derivatives resulted in the unexpected syntheses of other known PAN derivatives. Preparation of C-C PAN resulted in the synthesis of Fremy’s PAN as a by-product. Synthesis of C-N PAN resulted in the synthesis of C-C PAN and Fremy’s PAN. Synthesis of N-O radical PAN resulted in the production of C-C PAN and Fremy’s PAN.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.130
Threshold uncertainty score0.664

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.194
Teacher spread0.187 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2021
Admission routes1
Has abstractyes

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