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Record W4389526881 · doi:10.1002/adfm.202309304

Crack‐Free Tungsten Fabricated via Laser Powder Bed Fusion Additive Manufacturing

2023· article· en· W4389526881 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueAdvanced Functional Materials · 2023
Typearticle
Languageen
FieldEngineering
TopicAdditive Manufacturing Materials and Processes
Canadian institutionsMcGill University
FundersNatural Sciences and Engineering Research Council of CanadaMcGill University
KeywordsMaterials scienceTungstenOxideArgonNitrogenDiffusionMelting pointGrain boundarySolubilityFusionOxygenChemical engineeringMicrostructureThermal diffusivityAnalytical Chemistry (journal)MetallurgyComposite materialPhysical chemistryThermodynamics

Abstract

fetched live from OpenAlex

Abstract Additive manufacturing of tungsten (W) is challenging due to its high melting point, high thermal conductivity, oxidation tendency, and brittleness from grain boundary (GB) oxides. In this study, the processing of W through laser powder bed fusion is investigated. Parts are fabricated under argon (Ar) and nitrogen (N 2 ) atmospheres using the same processing parameters. The part produced in Ar has cracks with oxide precipitates decorating the fractured GBs. On the other hand, crack‐free W samples are produced under N 2 atmosphere without any additional process modification. In both cases, the oxygen (O) content in the LPBF samples is similar to the starting powder. Interestingly, the analysis of the samples fabricated in nitrogen suggests that nitrogen is retained beyond the equilibrium solid solubility limit, while high‐resolution electron micrographs of fractured surfaces reveal reduced levels of oxides at GBs. Increased hardness for samples processed under N 2 atmosphere is observed. Density Functional Theory (DFT) calculations performed to study the influence of interstitial nitrogen on oxygen diffusion in W indicated a hindrance to O diffusion from the presence of dissolved N.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesInsufficient payload (model declined to judge)
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.013
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0060.002

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.011
GPT teacher head0.205
Teacher spread0.195 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it