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Record W4389785518 · doi:10.26434/chemrxiv-2023-x07wk

A Non-Steady-State Electric Circuit in Electrophoresis on Paper: Thermal Consideration of Electrophoretic Lateral-Flow Assays

2023· preprint· en· W4389785518 on OpenAlexafffund
Nikita A. Ivanov, Vasily G. Panferov, Sergey N. Krylov

Bibliographic record

VenueChemRxiv · 2023
Typepreprint
Languageen
FieldEngineering
TopicElectrowetting and Microfluidic Technologies
Canadian institutionsYork University
FundersNatural Sciences and Engineering Research Council of CanadaMinistry of Science and Higher Education of the Russian FederationYork University
KeywordsElectrophoresisSteady state (chemistry)Electric fieldElectric currentVoltageElectronic circuitHot spot (computer programming)Current (fluid)MechanicsElectrical resistivity and conductivityChemistryAnalytical Chemistry (journal)Materials scienceChromatographyElectrical engineeringThermodynamicsPhysics

Abstract

fetched live from OpenAlex

Non-steady-state behaviors are not expected in electric circuits that lack significant capacitance, inductivity, and/or active feedback. Here, we report that electrophoresis on paper (used to conduct/enhance paper-based assays) can create a non-steady-state electric circuit. We studied electrophoresis on 4-mm wide nitrocellulose-membrane strips utilized in lateral-flow immunoassays; the voltage was applied to strip termini immersed in reservoirs with a running buffer. If the total supplied power exceeded approximately 0.5 W, neither the electric current nor the temperature map reached their steady states on a multi-minute time scale. The current grew slowly to its maximum and then slowly decreased, and the temperature map evolved slowly, with one or more hot spots appearing and disappearing gradually in different positions on the strip. The slow evolution of a temperature map led to the occurrence of a terminal hot spot in which the strip burned. No chaotic behavior was observed, i.e., time dependences of both the current and temperature map were reproducible. We analyzed major processes involved in paper-based electrophoresis and explained the non-steady-state behavior. Unlike ordinary electric circuits with metal conductors, paper-based electrophoresis involves two slow processes: (i) intense buffer evaporation from hot spots and (ii) buffer supply from the reservoirs by an interplay of the capillary penetration and the electroosmotic flow. These processes affect heat generation and/or dissipation on the strip and, accordingly, the resistivity profile along the strip. The slow evolution of the resistivity profile is responsible for the non-steady-state behavior. Our work is the first detailed and conclusive study of heat maps in electrophoretically-enhanced LFA. We demonstrate spatiotemporal temperature distribution, which emphasizes the need for the empirical study of thermal behaviors due to the inability to create predictive quantitative models of the complex interplay of multiple processes, including evaporation.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.006
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0010.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0010.002
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.013
GPT teacher head0.209
Teacher spread0.196 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2023
Admission routes2
Has abstractyes

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