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Record W4390892438 · doi:10.1002/anie.202317414

Enhanced Charge Carrier Dynamics on Sb<sub>2</sub>Se<sub>3</sub> Photocathodes for Efficient Photoelectrochemical Nitrate Reduction to Ammonia

2024· article· en· W4390892438 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueAngewandte Chemie International Edition · 2024
Typearticle
Languageen
FieldChemical Engineering
TopicAmmonia Synthesis and Nitrogen Reduction
Canadian institutionsConcordia University
Fundersnot available
KeywordsPhotocathodeAmmonia productionAmmoniaFaraday efficiencyMaterials scienceNitrateElectrochemistryChemistryPhotochemistryInorganic chemistryElectrodePhysical chemistryPhysicsElectron

Abstract

fetched live from OpenAlex

Abstract Ammonia (NH 3 ) is recognized as a transportable carrier for renewable energy fuels. Photoelectrochemical nitrate reduction reaction (PEC NO 3 RR) offers a sustainable solution for nitrate‐rich wastewater treatment by directly converting solar energy to ammonia. In this study, we demonstrate the highly selective PEC ammonia production from NO 3 RR by constructing a CoCu/TiO 2 /Sb 2 Se 3 photocathode. The constructed CoCu/TiO 2 /Sb 2 Se 3 photocathode achieves an ammonia Faraday efficiency (FE) of 88.01 % at −0.2 V RHE and an ammonia yield as high as 15.91 μmol h −1 cm −2 at −0.3 V RHE with an excellent onset potential of 0.43 V RHE . Dynamics experiments and theoretical calculations have demonstrated that the CoCu/TiO 2 /Sb 2 Se 3 photocathode possesses high light absorption capacity, excellent carrier transfer capability, and high charge separation and transfer efficiencies. The photocathode can effectively adsorb the reactant NO 3 − and intermediate, and the CoCu co‐catalyst increases the maximum Gibbs free energy difference between NO 3 RR and HER. Meanwhile, the Co species enhances the spin density of Cu, and increases the density of states near the Fermi level in pdos, which results in a high PEC NO 3 RR activity on CoCu/TiO 2 /Sb 2 Se 3 . This work provides a new avenue for the feasibility of efficient PEC ammonia synthesis from nitrate‐rich wastewater.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.069
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.012
GPT teacher head0.253
Teacher spread0.241 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it