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Record W4393226065 · doi:10.1039/bk9781837672035-00069

Connection of thermodynamics and kinetics in oxidation reactions catalyzed by transition metals and oxides

2024· book-chapter· en· W4393226065 on OpenAlexaff
William Thomas Broomhead, Ya-Huei Cathy Chin

Bibliographic record

Venuenot available
Typebook-chapter
Languageen
FieldChemical Engineering
TopicCatalysis and Oxidation Reactions
Canadian institutionsUniversity of Toronto
Fundersnot available
KeywordsKineticsCatalysisConnection (principal bundle)ThermodynamicsTransition metalMaterials scienceChemistryPhysical chemistryPhysicsOrganic chemistryQuantum mechanicsMathematics

Abstract

fetched live from OpenAlex

This chapter examines the oxidation reactions of alcohols and alkanes on transition metal or metal oxide surfaces. The diverse sets of reactions, including oxidative dehydrogenation, partial oxidation, reforming, and combustion, occur over temperature and oxygen chemical potential ranges spanned over many orders of magnitude, but they share similar active site requirements and mechanistic events—the oxygen chemical potentials dictate the thermodynamically stable states of the surfaces and type of reactive oxygen, on which catalytic turnovers occur via the general cycles of reductant and oxidant activation, kinetically coupled together. The chapter begins with an exploration on the thermodynamics of a bulk metal–O2 system and its application as a first approximation on the oxide phase and oxygen storage capacity, as well as the driving force in oxide redox reactions, the latter being graphically captured in an Ellingham diagram. Aside from bulk properties, the thermochemical properties of individual lattice oxygen atoms in dispersed metal oxides, such as their vacancy formation enthalpies, are expected to depend on their local coordination sphere. Through case studies, the chapter explores the general mechanistic trends, especially how the thermochemical properties of the reactive oxygen atoms, either as chemisorbed oxygen or lattice oxygen, mediate the catalytic conversion of alcohols and alkanes, through altering the active site structures and/or the character and activation free energy of the kinetically relevant C–H bond scission transition states.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: none
Teacher disagreement score0.581
Threshold uncertainty score0.767

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.216
Teacher spread0.207 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations4
Published2024
Admission routes1
Has abstractyes

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