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Record W4396580114 · doi:10.26434/chemrxiv-2024-nmm8w

Exploring the stereochemistry-specific tendency for interdigitation in synthetic monomycoloyl glycerol analogs through molecular dynamics simulations

2024· preprint· en· W4396580114 on OpenAlexaff
Suvi Heinonen, Artturi Koivuniemi, Matthew Davies, Mikko Karttunen, Camilla Foged, Alex Bunker

Bibliographic record

VenueChemRxiv · 2024
Typepreprint
Languageen
FieldChemistry
TopicAnalytical Chemistry and Chromatography
Canadian institutionsWestern University
Fundersnot available
KeywordsGlycerolMolecular dynamicsDynamics (music)ChemistryStereochemistryComputational biologyBiochemistryComputational chemistryBiologyPhysics

Abstract

fetched live from OpenAlex

Synthetic monomycoloyl glycerol (MMG) analogs possess robust immunostimulatory activity and are investigated as adjuvants for subunit vaccines in preclinical and clinical studies. These synthetic lipids consist of a glycerol moiety attached to a corynomycolic acid. Previous experimental studies have shown that the stereochemistry of the lipid acid moiety affects whether the MMG analogs self-assemble into interdigitated or non-interdigitated structures below the main phase transition temperature (Tm). In this study, we elucidated possible thermodynamic mechanisms governing the phase behavior of MMG analogs by exploring their conformations, interactions, and dynamics using molecular dynamics (MD) simulations. We compared two analogs, MMG-1 and MMG-6, which differ only by the stereochemistry of the lipid acid moiety; the former has a configuration different from the natural MMG, and the latter displays a native-like stereochemistry. Three different membrane states were simulated: 1) a non-interdigitated single bilayer, 2) a non-interdigitated double bilayer, and 3) a fully interdigitated double bilayer. Our results indicate that the propensity for interdigitation of the MMG analogs is linked to the degree to which their hydrocarbon chains are ordered and oriented, and the extent of the intermolecular interactions in their hydrophilic region. This study demonstrates how MD simulations can enhance the molecular understanding of vaccine adjuvants.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Simulation or modeling · Consensus signal: Simulation or modeling
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.009
Threshold uncertainty score0.018

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0010.000
Scholarly communication0.0000.001
Open science0.0010.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.054
GPT teacher head0.279
Teacher spread0.224 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designSimulation or modeling
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2024
Admission routes1
Has abstractyes

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Same venueChemRxivSame topicAnalytical Chemistry and ChromatographyFrench-language works237,207