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Record W4396622446 · doi:10.1002/cjce.25289

Removal of Co(<scp>II</scp>) and various metal ions from the residue of the zinc plant through solvent extraction using both acid and neutral extractants

2024· article· en· W4396622446 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

venuePublished in a venue whose home country is Canada.
no affNo Canadian affiliation: this work is invisible to an affiliation-only frame.
No Canadian affiliation. An affiliation-only frame, the usual design, would never have seen this work. It is one of the works that make the case for inverting the frame.

Bibliographic record

VenueThe Canadian Journal of Chemical Engineering · 2024
Typearticle
Languageen
FieldEngineering
TopicExtraction and Separation Processes
Canadian institutionsnot available
Fundersnot available
KeywordsCobaltZincChemistryPhosphoric acidMetal ions in aqueous solutionExtraction (chemistry)ManganeseInorganic chemistryMetalSolventElectrowinningElectrolyteNuclear chemistryChromatographyOrganic chemistryElectrode

Abstract

fetched live from OpenAlex

Abstract The recovery of cobalt from secondary sources is a crucial issue in technology development, particularly for its numerous applications in various industries. Solvent extraction has proven an effective method for metallic ions separation from secondary sources. The main goal of this work was to study the separation of metals by solvent extraction technique from zinc plant leach waste. Initially, several extractants, including Cyanex 272, Cyanex 301, LIX 5640 H, Alamine 336, and tri‐n‐octylamine (TOA), were tested to treat the leach solution. It was discovered that the saponified extractant di‐(2‐ethylhexyl) phosphoric acid (D2EHPA) (10%) + tri‐n‐butyl phosphate (TBP) (10%) effectively eliminated interfering elements such as manganese, zinc, and iron, with extraction efficiencies of 95%, 98%, and 99.9%, respectively. To increase the concentration of cobalt in the purified solution, the cobalt recovery step was performed using various acids on the loaded organic phase. The best outcome was achieved using ammonium sulphate salt (1 M), which recovered about 50% of the cobalt present in the organic phase. The recovered cobalt was then subjected to the electrowinning process to produce cobalt metal of high purity. A cathodic current density of 100 A/m 2 was determined to be the optimal current for the electrolyte solution. Lastly, scanning electron microscope (SEM) and X‐ray fluorescence (XRF) analyses were carried out to examine the structure and purity of the resulting metallic cobalt, which was found to have a purity of 99.5%.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.032
Threshold uncertainty score0.313

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.018
GPT teacher head0.236
Teacher spread0.218 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it