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Record W4396818271 · doi:10.1107/s2053273323090022

Exploration of primary and secondary sphere coordination by unsymmetric pyrimidine sulfanyl and aminopyrazole ligands

2023· article· en· W4396818271 on OpenAlexaff
Louise N. Dawe, S. D. Joekar, Lana K. Hiscock, Kaycee Anoliefo, A. Hankins, Kenneth E. Maly, Peter Boyle

Bibliographic record

VenueActa Crystallographica Section A Foundations and Advances · 2023
Typearticle
Languageen
FieldMedicine
TopicMetal complexes synthesis and properties
Canadian institutionsWestern UniversityWilfrid Laurier University
Fundersnot available
KeywordsSulfanylPyrimidinePrimary (astronomy)ChemistryCoordination sphereStereochemistryCrystallographyPhysicsCrystal structure

Abstract

fetched live from OpenAlex

In our exploration of ligand systems that simultaneously incorporate three types of molecular affinity: (i) coordination of Lewis acids; (ii) intermolecular interactions with anions; and (iii) additional functional modalities, we have recently focused on two classes of unsymmetric molecules based on (a) aminopyrazole and (b) pyrimidine sulfanyl cores (Fig. 1).We have targeted this design strategy because a knowledge gap still exists with respect to controlling the directionality of weak intermolecular forces [1], which may be further complicated in the presence of stronger, competing forces [2].

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.898
Threshold uncertainty score0.458

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.030
GPT teacher head0.264
Teacher spread0.234 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2023
Admission routes1
Has abstractyes

Explore more

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