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Record W4399653995 · doi:10.21203/rs.3.rs-4380373/v1

A universal method for precise in situ control of stoichiometry and termination of epitaxial perovskite thin films

2024· preprint· en· W4399653995 on OpenAlexaff
B. A. Davidson, A. Yu. Petrov, Fengmiao Li, Rebecca Pons, Hyungki Shin, Chong Liu, Pietro Parisse, Piero Torelli, Georg Cristiani, Г. Логвенов, Gideok Kim, Xiaoxing Xi, E. Benckiser, Ke Zou

Bibliographic record

VenueResearch Square · 2024
Typepreprint
Languageen
FieldMaterials Science
TopicElectronic and Structural Properties of Oxides
Canadian institutionsUniversity of British Columbia
Fundersnot available
KeywordsStoichiometryHeterojunctionEpitaxyPerovskite (structure)Materials scienceThin filmDiffractionCondensed matter physicsChemical physicsNanotechnologyChemistryOpticsCrystallographyLayer (electronics)PhysicsOptoelectronicsPhysical chemistry

Abstract

fetched live from OpenAlex

<title>Abstract</title> The perovskite ABO3 structure forms the basis for a wide range of functional and quantum materials discussed in the literature, although applications so far have been limited in part because accurate control of film stoichiometry and the ability to precisely construct heterostructures continues to lag behind their conventional semiconductor counterparts. While layer-by-layer growth mode is often cited for perovskite films, most transition-metal perovskite oxides self-assemble via an energetically-favorable layer-inversion mechanism whose phenomenology we demonstrate can be exploited to precisely adjust the stoichiometry and surface termination at any point during growth. Layer inversion results in a universal behavior of the in situ electron diffraction rocking curves and diffracted-beam intensity oscillations during alternating A- and B-site shuttered growth for a wide range of polar and nonpolar surfaces. We present a model that permits unambiguous interpretation of the oscillations, providing for the first time a completely in situ method for precise relative and absolute calibration of multielemental A- and B-site fluxes at the percent level, and apply it to successfully grow a single-phase high-entropy oxide film.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.003
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.134
Threshold uncertainty score0.511

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0030.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.001
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.034
GPT teacher head0.380
Teacher spread0.346 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2024
Admission routes1
Has abstractyes

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