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Record W4400006103 · doi:10.1021/acs.jpca.4c03093

Millimeter-Wave and High-Resolution Infrared Spectroscopy of 3-Furonitrile

2024· article· en· W4400006103 on OpenAlexaff
William H. Styers, Maria A. Zdanovskaia, Brian J. Esselman, Andrew N. Owen, Samuel M. Kougias, Brant Billinghurst, Jianbao Zhao, Robert J. McMahon, R. Claude Woods

Bibliographic record

VenueThe Journal of Physical Chemistry A · 2024
Typearticle
Languageen
FieldChemistry
TopicMolecular Spectroscopy and Structure
Canadian institutionsCanadian Light Source (Canada)University of Saskatchewan
FundersDivision of Chemistry
KeywordsExtremely high frequencyInfraredHigh resolutionMillimeterSpectroscopyInfrared spectroscopyResolution (logic)PhysicsMaterials scienceRemote sensingOpticsAstronomyGeologyComputer scienceArtificial intelligence

Abstract

fetched live from OpenAlex

The rotational spectrum of 3-furonitrile has been collected from 85 to 500 GHz, spanning the most intense rotational transitions observable at room temperature. The large dipole moment imparted by the nitrile substituent confers substantial intensity to the rotational spectrum, enabling the observation of over 5600 new rotational transitions. Combined with previously published transitions, the available data set was least-squares fit to partial-octic, distorted-rotor A- and S-reduced Hamiltonian models with low statistical uncertainty (σ fit < 0.031 MHz) for the ground vibrational state. Similar to its isomer 2-furonitrile, the two lowest-energy vibrationally excited states of 3-furonitrile (ν 17, ν 24 ), which correspond to the in-plane and out-of-plane nitrile bending vibrations, form an a- and b- axis Coriolis-coupled dyad. Rotationally resolved infrared transitions (30–600 cm –1 ) and over 4200 pure rotational transitions for both ν 17 and ν 24 were fit to a partial-octic, Coriolis-coupled, two-state Hamiltonian with low statistical uncertainty (σ fit rot < 0.045 MHz, σ fit IR < 6.1 MHz). The least-squares fitting of these vibrationally excited states provides their accurate and precise vibrational frequencies (ν 17 = 168.193 164 8 (67) cm –1 and ν 24 = 169.635 831 5 (77) cm –1 ) and seven Coriolis-coupling terms ( G a, G a J, G a K, F bc, F bc K, G b, and F ac ). The two fundamental states exhibit a notably small energy gap (1.442 667 (10) cm –1 ) and an inversion of the relative energies of ν 17 and ν 24 compared to those of the isomer 2-furonitrile. The rotational frequencies and spectroscopic constants of 3-furonitrile that we present herein provide a sufficient basis for conducting radioastronomical searches for this molecule across the majority of the frequency range available to current radiotelescopes.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.011
Threshold uncertainty score0.398

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.233
Teacher spread0.227 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations3
Published2024
Admission routes1
Has abstractyes

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