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Record W4400930897 · doi:10.1002/cjce.25412

Crude oil removal from water: Influence of organic phase composition and mineral content

2024· article· en· W4400930897 on OpenAlexvenueno aff
Ignacio Rintoul, Thomas Uldry, David Hunkeler

Bibliographic record

VenueThe Canadian Journal of Chemical Engineering · 2024
Typearticle
Languageen
FieldEngineering
TopicEnhanced Oil Recovery Techniques
Canadian institutionsnot available
Fundersnot available
KeywordsChemistryFlocculationTurbidityAqueous two-phase systemZincMineral oilSalt (chemistry)Aqueous solutionEnvironmental chemistryOrganic chemistry

Abstract

fetched live from OpenAlex

Abstract The effect of organic and inorganic compounds, commonly present in the mineralogy of crude oil and/or added in the washing processes of extracted crude, on the removal efficiency of emulsified oils present in waste washing waters was investigated by means of flocculation. Approximately 90% of the emulsified oil could be removed using an anionic flocculant, providing a residual turbidity below 100 NTU. The yield depended on the nature of the organic and inorganic components present. The higher the chain length of the main organic component, the greater the flocculant concentration required to remove the oil. Several components had an effect of emulsification (e.g., octane, decane), some of which rendered de‐oiling process completely ineffective (e.g., naphthenic acids). Aliphatics were the most difficult to eliminate, requiring flocculant levels in the 200–300 ppm range. This is in contrast to 75–100 ppm levels which were required to remove bi‐ and poly‐cyclic aromatics. Heavy oils were more difficult to remove than light oils. There was a strong effect of the pH of the aqueous phase. The optimum was pH = 2.0. Virtually all inorganic compounds reduced the efficiency of removing oil from water when spiked at 1%. The only exception was sodium carbonate which acted as a de‐emulsifier. Monovalent salts have a minor effect on de‐oiling, with efficiencies remaining at 80%. Divalent chlorides reduced the de‐oiling efficiency to 70% while sulphates had a more severe influence. The de‐oiling efficiency was lowered substantially with the addition of clays, zinc, cadmium, ferric oxide, calcium carbonate, and dibenyhlthiophene.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.006
Threshold uncertainty score0.012

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.195
Teacher spread0.187 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations2
Published2024
Admission routes1
Has abstractyes

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